5-(4-trifluoromethoxyphenyl)-3-(4-tetrahydropyranyl)imino-2-(2-methoxy-3-pyridyl)amino-3,5-dihydrophenazine

Base Information

Chemical Name:5-(4-trifluoromethoxyphenyl)-3-(4-tetrahydropyranyl)imino-2-(2-methoxy-3-pyridyl)amino-3,5-dihydrophenazine
CAS No.:1353734-14-1
Molecular Formula:C₃₀H₂₆F₃N₅O₃
Molecular Weight:561.563
Hs Code.:

Synonyms:5-(4-trifluoromethoxyphenyl)-3-(4-tetrahydropyranyl)imino-2-(2-methoxy-3-pyridyl)amino-3,5-dihydrophenazine

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Chemical Property of 5-(4-trifluoromethoxyphenyl)-3-(4-tetrahydropyranyl)imino-2-(2-methoxy-3-pyridyl)amino-3,5-dihydrophenazine

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Technology Process of 5-(4-trifluoromethoxyphenyl)-3-(4-tetrahydropyranyl)imino-2-(2-methoxy-3-pyridyl)amino-3,5-dihydrophenazine

There total 9 articles about 5-(4-trifluoromethoxyphenyl)-3-(4-tetrahydropyranyl)imino-2-(2-methoxy-3-pyridyl)amino-3,5-dihydrophenazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.2%

: 38041-19-9
4-aminotetrahydropyran

: C₂₅H₁₈F₃N₅O₂

: 1353734-14-1
5-(4-trifluoromethoxyphenyl)-3-(4-tetrahydropyranyl)imino-2-(2-methoxy-3-pyridyl)amino-3,5-dihydrophenazine

Guidance literature:: With acetic acid; In 1,4-dioxane; at 110 ℃;
DOI:10.1021/jm300828h

Reference yield:

: C₁₉H₁₂F₄N₄O₅

: 1353734-14-1
5-(4-trifluoromethoxyphenyl)-3-(4-tetrahydropyranyl)imino-2-(2-methoxy-3-pyridyl)amino-3,5-dihydrophenazine

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / tetrahydrofuran / Reflux

2: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; methanol / 20 °C / 2068.65 Torr

3: air / methanol / 20 °C

4: acetic acid / 1,4-dioxane / 110 °C

With palladium 10% on activated carbon; hydrogen; acetic acid; triethylamine; In tetrahydrofuran; 1,4-dioxane; methanol;
DOI:10.1021/jm300828h

Reference yield:

: C₂₅H₁₉F₃N₆O₆

: 1353734-14-1
5-(4-trifluoromethoxyphenyl)-3-(4-tetrahydropyranyl)imino-2-(2-methoxy-3-pyridyl)amino-3,5-dihydrophenazine

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; methanol / 20 °C / 2068.65 Torr

2: air / methanol / 20 °C

3: acetic acid / 1,4-dioxane / 110 °C

With palladium 10% on activated carbon; hydrogen; acetic acid; In tetrahydrofuran; 1,4-dioxane; methanol;
DOI:10.1021/jm300828h