13,37-Bis(methoxycarbonyl)-9,18,33,42-tetrakis(4-methoxyphenylsulfonyl)-1,2,9,18,25,26,33,42-octaaza<2.2.2.2.2.2>(1,3)cyclophan-1,25-dien

Base Information

Chemical Name:13,37-Bis(methoxycarbonyl)-9,18,33,42-tetrakis(4-methoxyphenylsulfonyl)-1,2,9,18,25,26,33,42-octaaza<2.2.2.2.2.2>(1,3)cyclophan-1,25-dien
CAS No.:140661-45-6
Molecular Formula:C₇₂H₆₄N₈O₁₆S₄
Molecular Weight:1425.61
Hs Code.:

Synonyms:13,37-Bis(methoxycarbonyl)-9,18,33,42-tetrakis(4-methoxyphenylsulfonyl)-1,2,9,18,25,26,33,42-octaaza<2.2.2.2.2.2>(1,3)cyclophan-1,25-dien

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Chemical Property of 13,37-Bis(methoxycarbonyl)-9,18,33,42-tetrakis(4-methoxyphenylsulfonyl)-1,2,9,18,25,26,33,42-octaaza<2.2.2.2.2.2>(1,3)cyclophan-1,25-dien

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Technology Process of 13,37-Bis(methoxycarbonyl)-9,18,33,42-tetrakis(4-methoxyphenylsulfonyl)-1,2,9,18,25,26,33,42-octaaza<2.2.2.2.2.2>(1,3)cyclophan-1,25-dien

There total 3 articles about 13,37-Bis(methoxycarbonyl)-9,18,33,42-tetrakis(4-methoxyphenylsulfonyl)-1,2,9,18,25,26,33,42-octaaza<2.2.2.2.2.2>(1,3)cyclophan-1,25-dien which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 29333-41-3
methyl 3,5-bis(bromomethyl)benzoate

: 140661-33-2
3,3'-Bis<(4-methoxyphenylsulfonyl)amino>azobenzol

: 140661-45-6
13,37-Bis(methoxycarbonyl)-9,18,33,42-tetrakis(4-methoxyphenylsulfonyl)-1,2,9,18,25,26,33,42-octaaza<2.2.2.2.2.2>(1,3)cyclophan-1,25-dien

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 40 ℃; for 12h;

Reference yield:

: 21371-44-8,140661-36-5
3,3'-diaminoazobenzene

: 140661-45-6
13,37-Bis(methoxycarbonyl)-9,18,33,42-tetrakis(4-methoxyphenylsulfonyl)-1,2,9,18,25,26,33,42-octaaza<2.2.2.2.2.2>(1,3)cyclophan-1,25-dien

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / pyridine / 2 h / 70 °C

2: 26 percent / Cs₂CO₃ / dimethylformamide / 12 h / 40 °C

With pyridine; caesium carbonate; In N,N-dimethyl-formamide;

Reference yield:

: 98-68-0
4-methoxy-phenyl-sulphonyl chloride

: 140661-45-6
13,37-Bis(methoxycarbonyl)-9,18,33,42-tetrakis(4-methoxyphenylsulfonyl)-1,2,9,18,25,26,33,42-octaaza<2.2.2.2.2.2>(1,3)cyclophan-1,25-dien

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / pyridine / 2 h / 70 °C

2: 26 percent / Cs₂CO₃ / dimethylformamide / 12 h / 40 °C

With pyridine; caesium carbonate; In N,N-dimethyl-formamide;