5-azido-3-O-benzyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-β-L-idofuranose

Base Information

Chemical Name:5-azido-3-O-benzyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-β-L-idofuranose
CAS No.:117383-74-1
Molecular Formula:C₃₅H₃₅N₃O₅
Molecular Weight:577.68
Hs Code.:

Synonyms:5-azido-3-O-benzyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-β-L-idofuranose

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Chemical Property of 5-azido-3-O-benzyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-β-L-idofuranose

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Technology Process of 5-azido-3-O-benzyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-β-L-idofuranose

There total 5 articles about 5-azido-3-O-benzyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-β-L-idofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 100-39-0
benzyl bromide

: 250128-84-8
5-azido-5-deoxy-1,2-O-isopropylidene-6-O-triphenylmethyl-β-L-idofuranose

: 117383-74-1
5-azido-3-O-benzyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-β-L-idofuranose

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.666667h;
DOI:10.1016/j.tet.2007.05.085

Reference yield:

: 117415-12-0
Trifluoro-methanesulfonic acid (R)-1-((3aR,5S,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-2-trityloxy-ethyl ester

: 117383-74-1
5-azido-3-O-benzyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-β-L-idofuranose

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)82028-6

Reference yield:

: 76-83-5
trityl chloride

: 117383-74-1
5-azido-3-O-benzyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-β-L-idofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / pyridine / 24 h / 20 °C

2: 80 percent / NaH / dimethylformamide / 0.67 h / 20 °C

With pyridine; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2007.05.085