5-azido-5-deoxy-1,2-O-isopropylidene-6-O-triphenylmethyl-β-L-idofuranose

Base Information

Chemical Name:5-azido-5-deoxy-1,2-O-isopropylidene-6-O-triphenylmethyl-β-L-idofuranose
CAS No.:250128-84-8
Molecular Formula:C₂₈H₂₉N₃O₅
Molecular Weight:487.555
Hs Code.:

Synonyms:5-azido-5-deoxy-1,2-O-isopropylidene-6-O-triphenylmethyl-β-L-idofuranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-azido-5-deoxy-1,2-O-isopropylidene-6-O-triphenylmethyl-β-L-idofuranose

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Technology Process of 5-azido-5-deoxy-1,2-O-isopropylidene-6-O-triphenylmethyl-β-L-idofuranose

There total 1 articles about 5-azido-5-deoxy-1,2-O-isopropylidene-6-O-triphenylmethyl-β-L-idofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 76-83-5
trityl chloride

: 130619-55-5
5-azido-5-deoxy-1,2-O-isopropylidene-β-L-idofuranose

: 250128-84-8
5-azido-5-deoxy-1,2-O-isopropylidene-6-O-triphenylmethyl-β-L-idofuranose

Guidance literature:: In pyridine; at 40 - 50 ℃; for 48h;
DOI:10.1016/S0008-6215(99)00119-6

Reference yield: 80.0%

: 100-39-0
benzyl bromide

: 250128-84-8
5-azido-5-deoxy-1,2-O-isopropylidene-6-O-triphenylmethyl-β-L-idofuranose

: 117383-74-1
5-azido-3-O-benzyl-5-deoxy-1,2-O-isopropylidene-6-O-trityl-β-L-idofuranose

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.666667h;
DOI:10.1016/j.tet.2007.05.085

Reference yield: 68.0%

: 250128-84-8
5-azido-5-deoxy-1,2-O-isopropylidene-6-O-triphenylmethyl-β-L-idofuranose

: 250128-87-1
5-azido-5-deoxy-1,2-O-isopropylidene-6-O-triphenylmethyl-β-L-lyxo-hex-3-ulofuranose

Guidance literature:: With 3 A molecular sieve; sodium acetate; pyridinium chlorochromate; In dichloromethane; Heating;
DOI:10.1016/S0008-6215(99)00119-6