4-(benzyloxycarbonylamino)-2,2,6,6-tetramethyl-4-(4-nitrophenyloxycarbonyl)-piperidine-1-oxyl

Base Information

Chemical Name:4-(benzyloxycarbonylamino)-2,2,6,6-tetramethyl-4-(4-nitrophenyloxycarbonyl)-piperidine-1-oxyl
CAS No.:139494-15-8
Molecular Formula:C₂₄H₂₈N₃O₇
Molecular Weight:470.502
Hs Code.:

Synonyms:4-(benzyloxycarbonylamino)-2,2,6,6-tetramethyl-4-(4-nitrophenyloxycarbonyl)-piperidine-1-oxyl

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Chemical Property of 4-(benzyloxycarbonylamino)-2,2,6,6-tetramethyl-4-(4-nitrophenyloxycarbonyl)-piperidine-1-oxyl

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Technology Process of 4-(benzyloxycarbonylamino)-2,2,6,6-tetramethyl-4-(4-nitrophenyloxycarbonyl)-piperidine-1-oxyl

There total 3 articles about 4-(benzyloxycarbonylamino)-2,2,6,6-tetramethyl-4-(4-nitrophenyloxycarbonyl)-piperidine-1-oxyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 7693-46-1
4-Nitrophenyl chloroformate

: 139494-09-0
4-(benzyloxycarbonylamino)-4-carboxy-2,2,6,6-tetramethylpiperidine-1-oxyl

: 139494-15-8
4-(benzyloxycarbonylamino)-2,2,6,6-tetramethyl-4-(4-nitrophenyloxycarbonyl)-piperidine-1-oxyl

Guidance literature:: With triethylamine; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide; for 1h; Ambient temperature;

Reference yield:

: 15871-57-5
4-Amino-4-carboxy-2,2,6,6-tetramethylpiperidine-1-oxyl radical

: 139494-15-8
4-(benzyloxycarbonylamino)-2,2,6,6-tetramethyl-4-(4-nitrophenyloxycarbonyl)-piperidine-1-oxyl

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / NaHCO₃ / H₂O / 4 h / Ambient temperature

2: 85 percent / Et₃N / CHCl₃; tetrahydrofuran; dimethylformamide / 1 h / Ambient temperature

With sodium hydrogencarbonate; triethylamine; In tetrahydrofuran; chloroform; water; N,N-dimethyl-formamide;

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 139494-15-8
4-(benzyloxycarbonylamino)-2,2,6,6-tetramethyl-4-(4-nitrophenyloxycarbonyl)-piperidine-1-oxyl

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / NaHCO₃ / H₂O / 4 h / Ambient temperature

2: 85 percent / Et₃N / CHCl₃; tetrahydrofuran; dimethylformamide / 1 h / Ambient temperature

With sodium hydrogencarbonate; triethylamine; In tetrahydrofuran; chloroform; water; N,N-dimethyl-formamide;