N-benzyloxycarbonyl-(2S)-aminobutyryl-(2R/S)-perhydroazepinecarboxylic acid

Base Information

Chemical Name:N-benzyloxycarbonyl-(2S)-aminobutyryl-(2R/S)-perhydroazepinecarboxylic acid
CAS No.:869307-76-6
Molecular Formula:C₁₉H₂₆N₂O₅
Molecular Weight:362.426
Hs Code.:

Synonyms:N-benzyloxycarbonyl-(2S)-aminobutyryl-(2R/S)-perhydroazepinecarboxylic acid

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Chemical Property of N-benzyloxycarbonyl-(2S)-aminobutyryl-(2R/S)-perhydroazepinecarboxylic acid

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Technology Process of N-benzyloxycarbonyl-(2S)-aminobutyryl-(2R/S)-perhydroazepinecarboxylic acid

There total 3 articles about N-benzyloxycarbonyl-(2S)-aminobutyryl-(2R/S)-perhydroazepinecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 869307-75-5
N-benzyloxycarbonyl-(2S)-aminobutyric acid 3,4-dihydro-4-oxo-1,2,3-benzotriazine ester

: 5227-53-2
(2R/S)-azepinecarboxylic acid

: 869307-76-6
N-benzyloxycarbonyl-(2S)-aminobutyryl-(2R/S)-perhydroazepinecarboxylic acid

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 120h;
DOI:10.1021/jm0500830

Reference yield:

: (7R,10R)-10-tert-butyl-9-methyl-1,9-diazabicyclo[5.3.0]decan-8-one

: 869307-76-6
N-benzyloxycarbonyl-(2S)-aminobutyryl-(2R/S)-perhydroazepinecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 34 percent / aq. HCl / 3 h / 180 °C

2: 100 percent / Et₃N / dimethylformamide / 120 h / 20 °C

With hydrogenchloride; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/jm0500830

Reference yield:

: 42918-86-5,1145-79-5,2900-20-1,20395-87-3
(S)-2-(((benzyloxy)carbonyl)amino)butanoic acid

: 869307-76-6
N-benzyloxycarbonyl-(2S)-aminobutyryl-(2R/S)-perhydroazepinecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / dicyclohexylcarbodiimide / tetrahydrofuran / 3 h / 20 °C

2: 100 percent / Et₃N / dimethylformamide / 120 h / 20 °C

With triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm0500830