3,7-dibromo dibenzoborole

Base Information

• Chemical Name: 3,7-dibromo dibenzoborole
• CAS No.: 454182-34-4
• Molecular Formula: C₂₉H₃₃BBr₂O₂
• Molecular Weight: 584.199
• Mol file: 454182-34-4.mol

Synonyms:3,7-dibromo dibenzoborole

Chemical Property of 3,7-dibromo dibenzoborole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,7-dibromo dibenzoborole

There total 1 articles about 3,7-dibromo dibenzoborole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

2,4,6-triisopropylphenylboronic acid dimethyl ester (145434-22-6) + 4,4′-dibromo-2,2′-diiodo-5,5′-dimethoxy-1,1′-biphenyl (454182-36-6) → 3,7-dibromo dibenzoborole (454182-34-4)

Guidance literature:

4,4′-dibromo-2,2′-diiodo-5,5′-dimethoxy-1,1′-biphenyl; With magnesium; In tetrahydrofuran;

2,4,6-triisopropylphenylboronic acid dimethyl ester; In tetrahydrofuran; Further stages.;

DOI:10.1021/ja026689k

Reference yield: 47.0%

1,2-Diiodoethane (624-73-7) + 3,7-dibromo dibenzoborole (454182-34-4) → 3,7-diiodo dibenzoborole (454182-35-5)

Guidance literature:

With tert.-butyl lithium; In diethyl ether; addn. ether soln. of ter-butyl lithium (4.4 mol. amt) to dibromo dibenzoborole, addn. ICH2CH2I.;

DOI:10.1021/ja026689k

Reference yield: 47.0%

3,7-dibromo dibenzoborole (454182-34-4) → 3,7-diiodo dibenzoborole (454182-35-5)

Guidance literature:

3,7-dibromo dibenzoborole; With tert.-butyl lithium; In diethyl ether;

With 1,2-Diiodoethane; In diethyl ether; Further stages.;

DOI:10.1021/ja026689k

upstream raw materials:

2,4,6-triisopropylphenylboronic acid dimethyl ester

4,4′-dibromo-2,2′-diiodo-5,5′-dimethoxy-1,1′-biphenyl

Downstream raw materials:

3,7-diiodo dibenzoborole

5-(2,4,6-triisopropylphenyl)-2,8-dimethoxy-3,7-di(2-thienyl)-5H-dibenzo[b,d]borole

(C₆H₂(OCH₃)(C₄H₂SC₄H₃S))2BC₆H₂(CH₃CHCH₃)3

5-(2,4,6-triisopropylphenyl)-2,8-dimethoxy-3,7-bis[p-(N,N-diphenylamino)phenyl]-5H-dibenzo[b,d]borole