C₆F₄B₂(C₆F₅)2C₆F₄CH₃CN

Base Information

• Chemical Name: C₆F₄B₂(C₆F₅)2C₆F₄CH₃CN
• CAS No.: 473712-76-4
• Molecular Formula: C₂₆H₃B₂F₁₈N
• Molecular Weight: 692.91
• Mol file: 473712-76-4.mol

Synonyms:C₆F₄B₂(C₆F₅)2C₆F₄CH₃CN

Chemical Property of C₆F₄B₂(C₆F₅)2C₆F₄CH₃CN

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆F₄B₂(C₆F₅)2C₆F₄CH₃CN

There total 4 articles about C₆F₄B₂(C₆F₅)2C₆F₄CH₃CN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

9,10-bis(pentafluorophenyl)perfluoro-9,10-diboraanthracene (220503-31-1) + tris(perfluorophenyl)borane-acetonitrile adduct (212619-93-7) → C6F4B2(C6F5)2C6F4CH3CN (473712-76-4)

Guidance literature:

In ⁽²⁾H₈-toluene; the mixt. in toluene-d7 was allowed to stand for 1 week at room temp. (N2); elem. anal.;

DOI:10.1021/om020079b

Reference yield:

9,10-bis(pentafluorophenyl)perfluoro-9,10-diboraanthracene (220503-31-1) + tris(perfluorophenyl)borane-acetonitrile adduct (212619-93-7) → C6F4B2(C6F5)2C6F4CH3CN (473712-76-4) + tris(pentafluorophenyl)borate (1109-15-5)

Guidance literature:

In ⁽²⁾H₈-toluene; the mixt. in toluene-d7 allowed to equilibrate for 1 h, from 40°Cto -47°C; not sepd., detected by NMR spectra;

DOI:10.1021/om020079b

Reference yield:

9,10-dichloro-1,2,3,4,5,6,7,8-octafluoro-9,10-dihydro-9,10-dibora-anthracene → C6F4B2(C6F5)2C6F4CH3CN (473712-76-4)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene

2: ⁽²⁾H₈-toluene

In ⁽²⁾H₈-toluene; toluene;

DOI:10.1021/om020079b

upstream raw materials:

9,10-bis(pentafluorophenyl)perfluoro-9,10-diboraanthracene

tris(perfluorophenyl)borane-acetonitrile adduct

1,2-bis(trimethylstannyl)benzene