(S)-4-((4-(4-methoxybenzyloxy)butoxy)methyl)-2,2-dimethyl-1,3-dioxolane

Base Information Edit

Chemical Name:(S)-4-((4-(4-methoxybenzyloxy)butoxy)methyl)-2,2-dimethyl-1,3-dioxolane
CAS No.:1415037-54-5
Molecular Formula:C₁₈H₂₈O₅
Molecular Weight:324.417
Hs Code.:
Mol file:1415037-54-5.mol

Synonyms:(S)-4-((4-(4-methoxybenzyloxy)butoxy)methyl)-2,2-dimethyl-1,3-dioxolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-4-((4-(4-methoxybenzyloxy)butoxy)methyl)-2,2-dimethyl-1,3-dioxolane Edit

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Technology Process of (S)-4-((4-(4-methoxybenzyloxy)butoxy)methyl)-2,2-dimethyl-1,3-dioxolane

There total 2 articles about (S)-4-((4-(4-methoxybenzyloxy)butoxy)methyl)-2,2-dimethyl-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-(4-methoxybenzyloxy)butyl methanesulfonate

: 22323-82-6,36543-79-0
(S)-(+)-(2,2-dimethyl-[1,3]dioxolan-4-yl)methanol

: 1415037-54-5
(S)-4-((4-(4-methoxybenzyloxy)butoxy)methyl)-2,2-dimethyl-1,3-dioxolane

Guidance literature:: (S)-(+)-(2,2-dimethyl-[1,3]dioxolan-4-yl)methanol; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 1.5h; Inert atmosphere;

4-(4-methoxybenzyloxy)butyl methanesulfonate; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1039/c2cc36604e DOI:10.1039/c2cc36604e

Reference yield:

: 123731-28-2
4-(4-methoxybenzyloxy)butan-1-ol

: 1415037-54-5
(S)-4-((4-(4-methoxybenzyloxy)butoxy)methyl)-2,2-dimethyl-1,3-dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / tetrahydrofuran / 5 h / 0 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1.5 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

With sodium hydride; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c2cc36604e DOI:10.1039/c2cc36604e