ethyl 2--2-(2-bromo-4,5-dimethoxyphenyl)acetate

Base Information

Chemical Name:ethyl 2--2-(2-bromo-4,5-dimethoxyphenyl)acetate
CAS No.:154535-01-0
Molecular Formula:C₂₄H₂₉BrClNO₇
Molecular Weight:558.854
Hs Code.:

ethyl 2-<N-chloromethylcarbonyl N-2-(3,4-dimethoxyphenyl)ethylamino>-2-(2-bromo-4,5-dimethoxyphenyl)acetate

Synonyms:ethyl 2--2-(2-bromo-4,5-dimethoxyphenyl)acetate

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Chemical Property of ethyl 2--2-(2-bromo-4,5-dimethoxyphenyl)acetate

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Technology Process of ethyl 2--2-(2-bromo-4,5-dimethoxyphenyl)acetate

There total 4 articles about ethyl 2--2-(2-bromo-4,5-dimethoxyphenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 79-04-9
chloroacetyl chloride

: 154535-00-9
ethyl 2-<2-(3,4-dimethoxyphenyl)ethylamino>-2-(2-bromo-4,5-dimethoxyphenyl)acetate

: 154535-01-0
ethyl 2--2-(2-bromo-4,5-dimethoxyphenyl)acetate

Guidance literature:: With triethylamine; In dichloromethane; for 3h;
DOI:10.1002/jhet.5570300541

Reference yield:

: 91881-19-5
ethyl (2-bromo-4,5-dimethoxyphenyl)acetate

: 154535-01-0
ethyl 2--2-(2-bromo-4,5-dimethoxyphenyl)acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / N-bromosuccinimide, azobisisobutyronitrile / CCl₄ / 1 h / Heating

2: 95 percent / triethylamine / CH₂Cl₂ / 1 h / Ambient temperature

3: 93 percent / triethylamine / CH₂Cl₂ / 3 h

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); triethylamine; In tetrachloromethane; dichloromethane;
DOI:10.1002/jhet.5570300541

Reference yield:

: 18066-68-7
ethyl 3,4-dimethoxyphenylacetate

: 154535-01-0
ethyl 2--2-(2-bromo-4,5-dimethoxyphenyl)acetate

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / N-bromosuccinimide, hydrobromic acid / CCl₄ / 0.83 h / 40 °C

2: 97 percent / N-bromosuccinimide, azobisisobutyronitrile / CCl₄ / 1 h / Heating

3: 95 percent / triethylamine / CH₂Cl₂ / 1 h / Ambient temperature

4: 93 percent / triethylamine / CH₂Cl₂ / 3 h

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); hydrogen bromide; triethylamine; In tetrachloromethane; dichloromethane;
DOI:10.1002/jhet.5570300541