Technology Process of C32H41N3O6
There total 16 articles about C32H41N3O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
In
dichloromethane;
at 0 - 20 ℃;
for 20h;
DOI:10.1021/jm4002296
- Guidance literature:
-
Multi-step reaction with 10 steps
1: sodium carbonate / tetrahydrofuran; water / 36 h / 20 °C
2: hydrogenchloride / ethyl acetate; water; methanol / 2 h / 20 °C
3: Dess-Martin periodane / dichloromethane / 2 h / 20 °C
4: sodium chlorite; sodium dihydrogen phosphate dihydrate; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol / 5 h / 20 °C
5: triethylamine; diphenyl phosphoryl azide / dichloromethane / 15.33 h / 0 - 20 °C
6: 17 h / Reflux
7: potassium carbonate; methanol / 23 h / 20 °C
8: triethylamine / dichloromethane / 17 h / 0 - 20 °C
9: trifluoroacetic acid / dichloromethane / 0.17 h / 20 °C
10: triethylamine / dichloromethane / 20 h / 0 - 20 °C
With
hydrogenchloride; methanol; sodium chlorite; 2-methyl-but-2-ene; sodium dihydrogen phosphate dihydrate; diphenyl phosphoryl azide; sodium carbonate; potassium carbonate; Dess-Martin periodane; triethylamine; trifluoroacetic acid;
In
tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; tert-butyl alcohol;
DOI:10.1021/jm4002296
- Guidance literature:
-
Multi-step reaction with 9 steps
1: hydrogenchloride / ethyl acetate; water; methanol / 2 h / 20 °C
2: Dess-Martin periodane / dichloromethane / 2 h / 20 °C
3: sodium chlorite; sodium dihydrogen phosphate dihydrate; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol / 5 h / 20 °C
4: triethylamine; diphenyl phosphoryl azide / dichloromethane / 15.33 h / 0 - 20 °C
5: 17 h / Reflux
6: potassium carbonate; methanol / 23 h / 20 °C
7: triethylamine / dichloromethane / 17 h / 0 - 20 °C
8: trifluoroacetic acid / dichloromethane / 0.17 h / 20 °C
9: triethylamine / dichloromethane / 20 h / 0 - 20 °C
With
hydrogenchloride; methanol; sodium chlorite; 2-methyl-but-2-ene; sodium dihydrogen phosphate dihydrate; diphenyl phosphoryl azide; potassium carbonate; Dess-Martin periodane; triethylamine; trifluoroacetic acid;
In
tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; tert-butyl alcohol;
DOI:10.1021/jm4002296