N⁵-benzyl-N¹,N⁹-bis(2,3-dimethoxybenzoyl)bis(4-aminobutyl)amine hydrochloride

Base Information

Chemical Name:N⁵-benzyl-N¹,N⁹-bis(2,3-dimethoxybenzoyl)bis(4-aminobutyl)amine hydrochloride
CAS No.:78217-73-9
Molecular Formula:C₃₃H₄₃N₃O₆*ClH
Molecular Weight:614.182
Hs Code.:

N<sup>5</sup>-benzyl-N<sup>1</sup>,N<sup>9</sup>-bis(2,3-dimethoxybenzoyl)bis(4-aminobutyl)amine hydrochloride

Synonyms:N⁵-benzyl-N¹,N⁹-bis(2,3-dimethoxybenzoyl)bis(4-aminobutyl)amine hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N⁵-benzyl-N¹,N⁹-bis(2,3-dimethoxybenzoyl)bis(4-aminobutyl)amine hydrochloride

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Technology Process of N⁵-benzyl-N¹,N⁹-bis(2,3-dimethoxybenzoyl)bis(4-aminobutyl)amine hydrochloride

There total 3 articles about N⁵-benzyl-N¹,N⁹-bis(2,3-dimethoxybenzoyl)bis(4-aminobutyl)amine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 78217-68-2
N⁵-Benzylhomospermidine

: 7169-06-4
2,3-dimethoxybenzoyl chloride

: 78217-73-9
N⁵-benzyl-N¹,N⁹-bis(2,3-dimethoxybenzoyl)bis(4-aminobutyl)amine hydrochloride

Guidance literature:: With triethylamine; In dichloromethane; 0 deg C to room temperature;
DOI:10.1021/jo00335a041

Reference yield:

: 78217-67-1
N,N-Bis(3-cyanopropyl)-benzylamine

: 78217-73-9
N⁵-benzyl-N¹,N⁹-bis(2,3-dimethoxybenzoyl)bis(4-aminobutyl)amine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / LiAlH₄, AlCl₃

2: 97 percent / triethylamine / CH₂Cl₂ / 0 deg C to room temperature

With lithium aluminium tetrahydride; aluminium trichloride; triethylamine; In dichloromethane;
DOI:10.1021/jo00335a041

Reference yield:

: 100-46-9
benzylamine

: 78217-73-9
N⁵-benzyl-N¹,N⁹-bis(2,3-dimethoxybenzoyl)bis(4-aminobutyl)amine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / K₂CO₃ / butan-1-ol / 22 h / 115 °C

2: 66 percent / LiAlH₄, AlCl₃

3: 97 percent / triethylamine / CH₂Cl₂ / 0 deg C to room temperature

With lithium aluminium tetrahydride; aluminium trichloride; potassium carbonate; triethylamine; In dichloromethane; butan-1-ol;
DOI:10.1021/jo00335a041