4-<amino>tetradecachlorotriphenylmethyl radical

Base Information

Chemical Name:4-<amino>tetradecachlorotriphenylmethyl radical
CAS No.:65639-04-5
Molecular Formula:C₃₂H₁₆Cl₁₄N₃O₄
Molecular Weight:1002.84
Hs Code.:

4-<<N-(Benzyloxycarbonyl)alanylglycyl>amino>tetradecachlorotriphenylmethyl radical

Synonyms:4-<amino>tetradecachlorotriphenylmethyl radical

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Chemical Property of 4-<amino>tetradecachlorotriphenylmethyl radical

Chemical Property:

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Technology Process of 4-<amino>tetradecachlorotriphenylmethyl radical

There total 4 articles about 4-<amino>tetradecachlorotriphenylmethyl radical which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1142-20-7
N-Cbz-Ala

: 65639-05-6
Tetradecachloro-4-(glycylamino)triphenylmethyl radical hydrobromide

: 65638-92-8
4-<amino>tetradecachlorotriphenylmethyl radical

: 65639-04-5
4-<amino>tetradecachlorotriphenylmethyl radical

Guidance literature:: With chloroformic acid ethyl ester; triethylamine; 1.) CHCl₃, 0 deg C 10 min, 2.) CHCl₃, 0-10 deg C, 3h; room temp., 1.5h;
DOI:10.1021/jo00169a021

Reference yield:

: 64269-29-0
4-Aminotetradecachlorotriphenylmethyl Radical

: 65639-04-5
4-<amino>tetradecachlorotriphenylmethyl radical

Guidance literature:: Multi-step reaction with 3 steps

1: 30 percent / 1.) N,N-dimethylformamide, SOCl₂ / 1.) benzene, room temp., 2.) CHCl₃, 0 deg C; 30 min, room temp., 3.) CHCl₃, 4 days, room temp.

2: 99.8 percent / HBr / dioxane / 1 h / Ambient temperature

3: 64 percent / 1.) NEt₃, ethyl chloroformate, 2.) NEt₃ / 1.) CHCl₃, 0 deg C 10 min, 2.) CHCl₃, 0-10 deg C, 3h; room temp., 1.5h

With thionyl chloride; hydrogen bromide; chloroformic acid ethyl ester; triethylamine; N,N-dimethyl-formamide; In 1,4-dioxane;
DOI:10.1021/jo00169a021

Reference yield:

: 65639-03-4
4-<amino>tetradecachlorotriphenylmethyl Radical

: 65639-04-5
4-<amino>tetradecachlorotriphenylmethyl radical

Guidance literature:: Multi-step reaction with 2 steps

1: 99.8 percent / HBr / dioxane / 1 h / Ambient temperature

2: 64 percent / 1.) NEt₃, ethyl chloroformate, 2.) NEt₃ / 1.) CHCl₃, 0 deg C 10 min, 2.) CHCl₃, 0-10 deg C, 3h; room temp., 1.5h

With hydrogen bromide; chloroformic acid ethyl ester; triethylamine; In 1,4-dioxane;
DOI:10.1021/jo00169a021