C₂₉H₃₂N₂O₅S

Base Information

Chemical Name:C₂₉H₃₂N₂O₅S
CAS No.:1374108-58-3
Molecular Formula:C₂₉H₃₂N₂O₅S
Molecular Weight:520.649
Hs Code.:

C<sub>29</sub>H<sub>32</sub>N<sub>2</sub>O<sub>5</sub>S

Synonyms:C₂₉H₃₂N₂O₅S

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Chemical Property of C₂₉H₃₂N₂O₅S

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Technology Process of C₂₉H₃₂N₂O₅S

There total 5 articles about C₂₉H₃₂N₂O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 4124-41-8
p-toluenesulfonylanhydride

: 1374108-57-2
C₂₂H₂₆N₂O₃

: 1374108-58-3
C₂₉H₃₂N₂O₅S

Guidance literature:: With pyridine; In tetrahydrofuran; for 0.5h; Cooling with ice;

Reference yield:

: 15450-76-7
quinoline-2,8-diol

: 1374108-58-3
C₂₉H₃₂N₂O₅S

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride; N,N-dimethyl-formamide / 5.5 h / 20 - 50 °C / Cooling with ice

2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 16 h / 20 °C / Cooling with ice

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; 1,2-dimethoxyethane / 16 h / 80 °C / Inert atmosphere

4: hydrogenchloride / methanol; water / 1 h / 70 °C

5: pyridine / tetrahydrofuran / 0.5 h / Cooling with ice

With pyridine; hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; di-isopropyl azodicarboxylate; potassium carbonate; N,N-dimethyl-formamide; triphenylphosphine; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; water;

Reference yield:

: 1374108-55-0
C₁₅H₁₆ClNO₃

: 1374108-58-3
C₂₉H₃₂N₂O₅S

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; 1,2-dimethoxyethane / 16 h / 80 °C / Inert atmosphere

2: hydrogenchloride / methanol; water / 1 h / 70 °C

3: pyridine / tetrahydrofuran / 0.5 h / Cooling with ice

With pyridine; hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; water;