1-O-acetyl-4-azido-3-O-benzyl-2-O-bromoacetyl-4,6-dideoxy-D-glucopyranoside

Base Information

Chemical Name:1-O-acetyl-4-azido-3-O-benzyl-2-O-bromoacetyl-4,6-dideoxy-D-glucopyranoside
CAS No.:876345-23-2
Molecular Formula:C₁₇H₂₀BrN₃O₆
Molecular Weight:442.266
Hs Code.:

Synonyms:1-O-acetyl-4-azido-3-O-benzyl-2-O-bromoacetyl-4,6-dideoxy-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-O-acetyl-4-azido-3-O-benzyl-2-O-bromoacetyl-4,6-dideoxy-D-glucopyranoside

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Technology Process of 1-O-acetyl-4-azido-3-O-benzyl-2-O-bromoacetyl-4,6-dideoxy-D-glucopyranoside

There total 2 articles about 1-O-acetyl-4-azido-3-O-benzyl-2-O-bromoacetyl-4,6-dideoxy-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 876345-22-1
methyl 4-azido-3-O-benzyl-2-O-bromoacetyl-4,6-dideoxy-α-D-glucopyranoside

: 108-24-7
acetic anhydride

: 876345-23-2
1-O-acetyl-4-azido-3-O-benzyl-2-O-bromoacetyl-4,6-dideoxy-D-glucopyranoside

Guidance literature:: With sulfuric acid; acetic acid; at 20 ℃; for 1h;
DOI:10.1016/j.bmcl.2005.10.056

Reference yield:

: 861819-27-4
methyl 4-azido-3-O-benzyl-4,6-dideoxy-α-D-glucopyranoside

: 876345-23-2
1-O-acetyl-4-azido-3-O-benzyl-2-O-bromoacetyl-4,6-dideoxy-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / TMU / CH₂Cl₂ / 0 - 20 °C

2: 93 percent / H₂SO₄; AcOH / 1 h / 20 °C

With sulfuric acid; acetic acid; tetramethylurea; In dichloromethane;
DOI:10.1016/j.bmcl.2005.10.056