Dimethyl-dithiocarbamic acid 3-[2-(2-hydroxy-ethoxy)-phenoxy]-propyl ester

Base Information

Chemical Name:Dimethyl-dithiocarbamic acid 3-[2-(2-hydroxy-ethoxy)-phenoxy]-propyl ester
CAS No.:188121-14-4
Molecular Formula:C₁₄H₂₁NO₃S₂
Molecular Weight:315.458
Hs Code.:

Synonyms:Dimethyl-dithiocarbamic acid 3-[2-(2-hydroxy-ethoxy)-phenoxy]-propyl ester

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Chemical Property of Dimethyl-dithiocarbamic acid 3-[2-(2-hydroxy-ethoxy)-phenoxy]-propyl ester

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Technology Process of Dimethyl-dithiocarbamic acid 3-[2-(2-hydroxy-ethoxy)-phenoxy]-propyl ester

There total 4 articles about Dimethyl-dithiocarbamic acid 3-[2-(2-hydroxy-ethoxy)-phenoxy]-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 188120-97-0
[2-(3-bromopropoxy)phenoxy]ethanol

: 128-04-1
sodium dimethyldithiocarbamate

: 188121-14-4
Dimethyl-dithiocarbamic acid 3-[2-(2-hydroxy-ethoxy)-phenoxy]-propyl ester

Guidance literature:: In acetonitrile;

Reference yield:

: 4792-78-3
2-(2-hydroxy-phenoxy)-ethanol

: 188121-14-4
Dimethyl-dithiocarbamic acid 3-[2-(2-hydroxy-ethoxy)-phenoxy]-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / potassium carbonate / acetone / 24 h / Heating

2: 79 percent / acetonitrile

With potassium carbonate; In acetone; acetonitrile;

Reference yield:

: 18181-71-0
2-(2-methoxyphenoxy)ethanol

: 188121-14-4
Dimethyl-dithiocarbamic acid 3-[2-(2-hydroxy-ethoxy)-phenoxy]-propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / lithium diphenylphosphide, butyllithium / tetrahydrofuran / 3 h

2: 81 percent / potassium carbonate / acetone / 24 h / Heating

3: 79 percent / acetonitrile

With n-butyllithium; potassium carbonate; lithium diphenylphosphide; In tetrahydrofuran; acetone; acetonitrile;