Technology Process of 6,8-bis(phenylthio)-1,4-dimethoxy-7H-benzocyclohepten-6-one
There total 6 articles about 6,8-bis(phenylthio)-1,4-dimethoxy-7H-benzocyclohepten-6-one which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
N,N-dimethyl-formamide;
at 85 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: benzyl triethylammonium chloride, 20percent aq. K2CO3 / CH2Cl2 / 48 h / 45 - 50 °C
2: 50percent aq. ethanolic KOH / Heating
3: 1.) NaOEt, 2.) CH3ONa / 1.) EtOH, from 80 deg C to 90 deg C, overnight, 2.) EtOH, 90 deg C, 10 h
With
potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; sodium methylate; sodium ethanolate; potassium carbonate;
In
dichloromethane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 50percent aq. ethanolic KOH / Heating
2: 1.) NaOEt, 2.) CH3ONa / 1.) EtOH, from 80 deg C to 90 deg C, overnight, 2.) EtOH, 90 deg C, 10 h
With
potassium hydroxide; sodium methylate; sodium ethanolate;