1,4-bis-(N-benzoyl(thiocarbamoyl)amino)-1,4-dimethoxycarbonyl-cyclohexane

Base Information

Chemical Name:1,4-bis-(N-benzoyl(thiocarbamoyl)amino)-1,4-dimethoxycarbonyl-cyclohexane
CAS No.:896473-03-3
Molecular Formula:C₂₆H₂₈N₄O₆S₂
Molecular Weight:556.664
Hs Code.:

Synonyms:1,4-bis-(N-benzoyl(thiocarbamoyl)amino)-1,4-dimethoxycarbonyl-cyclohexane

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Chemical Property of 1,4-bis-(N-benzoyl(thiocarbamoyl)amino)-1,4-dimethoxycarbonyl-cyclohexane

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Technology Process of 1,4-bis-(N-benzoyl(thiocarbamoyl)amino)-1,4-dimethoxycarbonyl-cyclohexane

There total 5 articles about 1,4-bis-(N-benzoyl(thiocarbamoyl)amino)-1,4-dimethoxycarbonyl-cyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 896473-02-2
dimethyl trans-1,4-diaminocyclohexane-1,4-dicarboxylate

: 532-55-8
Benzoyl isothiocyanate

: 896473-03-3
1,4-bis-(N-benzoyl(thiocarbamoyl)amino)-1,4-dimethoxycarbonyl-cyclohexane

Guidance literature:: In dichloromethane; at 20 ℃; for 24h;
DOI:10.1016/j.tet.2006.03.038

Reference yield:

: 896472-99-4
1,4-diamino-cyclohexane-1,4-dicarboxylic acid

: 896473-03-3
1,4-bis-(N-benzoyl(thiocarbamoyl)amino)-1,4-dimethoxycarbonyl-cyclohexane

Guidance literature:: Multi-step reaction with 4 steps

1.1: diisopropylamine; chlorotrimethylsilane / CH₂Cl₂ / 4 h / Heating

1.2: 90 percent / CH₂Cl₂ / 20 °C

2.1: 93 percent / anhydrous K₂CO₃ / dimethylformamide / 48 h / 20 °C

3.1: 90.5 percent / H₂ / Pd/C / methanol / 1.5 h / 20 °C / 517.15 Torr

4.1: 95 percent / CH₂Cl₂ / 24 h / 20 °C

With chloro-trimethyl-silane; hydrogen; potassium carbonate; diisopropylamine; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2006.03.038

Reference yield:

: 1,3,9,11-tetraaza-dispiro[4.2.4.2]tetradecane-2,4,10,12-tetraone

: 896473-03-3
1,4-bis-(N-benzoyl(thiocarbamoyl)amino)-1,4-dimethoxycarbonyl-cyclohexane

Guidance literature:: Multi-step reaction with 5 steps

1.1: 65 percent / NaOH / H₂O / 16 h / 120 °C

2.1: diisopropylamine; chlorotrimethylsilane / CH₂Cl₂ / 4 h / Heating

2.2: 90 percent / CH₂Cl₂ / 20 °C

3.1: 93 percent / anhydrous K₂CO₃ / dimethylformamide / 48 h / 20 °C

4.1: 90.5 percent / H₂ / Pd/C / methanol / 1.5 h / 20 °C / 517.15 Torr

5.1: 95 percent / CH₂Cl₂ / 24 h / 20 °C

With sodium hydroxide; chloro-trimethyl-silane; hydrogen; potassium carbonate; diisopropylamine; palladium on activated charcoal; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2006.03.038