dimethyl trans-1,4-di(benzyloxycarbonylamino)cyclohexane-1,4-dicarboxylate

Base Information

Chemical Name:dimethyl trans-1,4-di(benzyloxycarbonylamino)cyclohexane-1,4-dicarboxylate
CAS No.:896473-01-1
Molecular Formula:C₂₆H₃₀N₂O₈
Molecular Weight:498.533
Hs Code.:

Synonyms:dimethyl trans-1,4-di(benzyloxycarbonylamino)cyclohexane-1,4-dicarboxylate

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Chemical Property of dimethyl trans-1,4-di(benzyloxycarbonylamino)cyclohexane-1,4-dicarboxylate

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Technology Process of dimethyl trans-1,4-di(benzyloxycarbonylamino)cyclohexane-1,4-dicarboxylate

There total 4 articles about dimethyl trans-1,4-di(benzyloxycarbonylamino)cyclohexane-1,4-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 896473-00-0
trans-1,4-di(benzyloxycarbonylamino)cyclohexane-1,4-dicarboxylic acid

: 74-88-4
methyl iodide

: 896473-01-1
dimethyl trans-1,4-di(benzyloxycarbonylamino)cyclohexane-1,4-dicarboxylate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 48h;
DOI:10.1016/j.tet.2006.03.038

Reference yield:

: C₂₄H₂₄N₂O₈^(2-)*2Cs⁽¹⁺⁾

: 74-88-4
methyl iodide

: 896473-01-1
dimethyl trans-1,4-di(benzyloxycarbonylamino)cyclohexane-1,4-dicarboxylate

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1021/jo901892d

Reference yield:

: 896472-99-4
1,4-diamino-cyclohexane-1,4-dicarboxylic acid

: 896473-01-1
dimethyl trans-1,4-di(benzyloxycarbonylamino)cyclohexane-1,4-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: diisopropylamine; chlorotrimethylsilane / CH₂Cl₂ / 4 h / Heating

1.2: 90 percent / CH₂Cl₂ / 20 °C

2.1: 93 percent / anhydrous K₂CO₃ / dimethylformamide / 48 h / 20 °C

With chloro-trimethyl-silane; potassium carbonate; diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2006.03.038