Technology Process of 3-aminocyclohex-2-enone hydrobromide
There total 2 articles about 3-aminocyclohex-2-enone hydrobromide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen bromide;
In
ethanol; water;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: acetic acid; ammonium acetate / benzene / 7 h / Reflux
2: hydrogen bromide / ethanol; water
With
ammonium acetate; hydrogen bromide; acetic acid;
In
ethanol; water; benzene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: ethanol / 9 h / Reflux
2.1: triphenylphosphine; palladium diacetate; potassium carbonate / acetonitrile / 0.25 - 0.33 h / 20 °C / Inert atmosphere
2.2: 4 h / Reflux; Inert atmosphere
3.1: sodium tetrahydroborate / water; tetrahydrofuran; methanol / 1 h / -5 - 0 °C
With
sodium tetrahydroborate; palladium diacetate; potassium carbonate; triphenylphosphine;
In
tetrahydrofuran; methanol; ethanol; water; acetonitrile;
2.1: |Sonogashira Cross-Coupling / 2.2: |Sonogashira Cross-Coupling;
