2,2-difluoro-1-(4-bromophenyl)-2-phenylsulfanyl-1-trimethoxysiloxyethane

Base Information

Chemical Name:2,2-difluoro-1-(4-bromophenyl)-2-phenylsulfanyl-1-trimethoxysiloxyethane
CAS No.:899820-47-4
Molecular Formula:C₁₇H₁₉BrF₂OSSi
Molecular Weight:417.39
Hs Code.:

Synonyms:2,2-difluoro-1-(4-bromophenyl)-2-phenylsulfanyl-1-trimethoxysiloxyethane

Suppliers and Price of 2,2-difluoro-1-(4-bromophenyl)-2-phenylsulfanyl-1-trimethoxysiloxyethane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,2-difluoro-1-(4-bromophenyl)-2-phenylsulfanyl-1-trimethoxysiloxyethane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,2-difluoro-1-(4-bromophenyl)-2-phenylsulfanyl-1-trimethoxysiloxyethane

There total 4 articles about 2,2-difluoro-1-(4-bromophenyl)-2-phenylsulfanyl-1-trimethoxysiloxyethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1122-91-4
4-bromo-benzaldehyde

: 536975-49-2
phenyl (trimethylsilyl)difluoromethyl sulfide

: 2,2-difluoro-1-(4-bromophenyl)-2-phenylsulfanylethanol

: 899820-47-4
2,2-difluoro-1-(4-bromophenyl)-2-phenylsulfanyl-1-trimethoxysiloxyethane

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1016/j.tet.2006.04.015

Reference yield:

: 1122-91-4
4-bromo-benzaldehyde

: 536975-49-2
phenyl (trimethylsilyl)difluoromethyl sulfide

: 899820-47-4
2,2-difluoro-1-(4-bromophenyl)-2-phenylsulfanyl-1-trimethoxysiloxyethane

Guidance literature:: With tetrabutylammonium triphenyldifluorosilicate; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1016/j.jfluchem.2004.12.005

Reference yield:

: 930-69-8
sodium thiophenolate

: 899820-47-4
2,2-difluoro-1-(4-bromophenyl)-2-phenylsulfanyl-1-trimethoxysiloxyethane

Guidance literature:: Multi-step reaction with 3 steps

1: dibenzo-18-crown-6 / diethyl ether

2: 85 percent / Mg / dimethylformamide

3: tetrabutylammonium triphenyldifluorosilicate / tetrahydrofuran / 0 - 20 °C

With dibenzo-18-crown-6; magnesium; tetrabutylammonium triphenyldifluorosilicate; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide; 2: Barbier coupling;
DOI:10.1016/j.jfluchem.2004.12.005