(1,1-bis(hydroxymethyl)propyl)carbamic acid phenyl ester

Base Information

Chemical Name:(1,1-bis(hydroxymethyl)propyl)carbamic acid phenyl ester
CAS No.:1346042-51-0
Molecular Formula:C₁₂H₁₇NO₄
Molecular Weight:239.271
Hs Code.:

Synonyms:(1,1-bis(hydroxymethyl)propyl)carbamic acid phenyl ester

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Chemical Property of (1,1-bis(hydroxymethyl)propyl)carbamic acid phenyl ester

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Technology Process of (1,1-bis(hydroxymethyl)propyl)carbamic acid phenyl ester

There total 4 articles about (1,1-bis(hydroxymethyl)propyl)carbamic acid phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 1885-14-9
phenyl chloroformate

: 115-70-8
2-ethyl-2-amino-propane-1,3-diol

: 1346042-51-0
(1,1-bis(hydroxymethyl)propyl)carbamic acid phenyl ester

Guidance literature:: With triethylamine; In acetonitrile; at 0 - 20 ℃; for 48h; Inert atmosphere;
DOI:10.1021/ol202430e

Reference yield:

: 1464781-72-3
C₁₅H₂₁NO₄

: 1346042-51-0
(1,1-bis(hydroxymethyl)propyl)carbamic acid phenyl ester

Guidance literature:: With acetic acid; In water; at 80 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c3cc45099f

Reference yield:

: 1033408-72-8
C₁₃H₂₅NO₄

: 1346042-51-0
(1,1-bis(hydroxymethyl)propyl)carbamic acid phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: trimethylsilyl trifluoromethanesulfonate; 2,6-dimethylpyridine / dichloromethane / -78 °C / Inert atmosphere; Cooling with ice

1.2: Inert atmosphere

2.1: triethylamine / dichloromethane / 1 h / Inert atmosphere; Cooling with ice

3.1: acetic acid / water / 1 h / 80 °C / Inert atmosphere

With 2,6-dimethylpyridine; trimethylsilyl trifluoromethanesulfonate; acetic acid; triethylamine; In dichloromethane; water;
DOI:10.1039/c3cc45099f