(S)-tert-butyl 2-((1-(4-methoxy-2,6-dimethylphenylsulfonyl)pyrrolidin-2-yl)methoxy)acetate

Base Information

Chemical Name:(S)-tert-butyl 2-((1-(4-methoxy-2,6-dimethylphenylsulfonyl)pyrrolidin-2-yl)methoxy)acetate
CAS No.:1190971-06-2
Molecular Formula:C₂₀H₃₁NO₆S
Molecular Weight:413.535
Hs Code.:

Synonyms:(S)-tert-butyl 2-((1-(4-methoxy-2,6-dimethylphenylsulfonyl)pyrrolidin-2-yl)methoxy)acetate

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Chemical Property of (S)-tert-butyl 2-((1-(4-methoxy-2,6-dimethylphenylsulfonyl)pyrrolidin-2-yl)methoxy)acetate

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Technology Process of (S)-tert-butyl 2-((1-(4-methoxy-2,6-dimethylphenylsulfonyl)pyrrolidin-2-yl)methoxy)acetate

There total 5 articles about (S)-tert-butyl 2-((1-(4-methoxy-2,6-dimethylphenylsulfonyl)pyrrolidin-2-yl)methoxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 5292-43-3
bromoacetic acid tert-butyl ester

: 1056629-16-3
(S)-(1-(4-methoxy-2,6-dimethylphenylsulfonyl)pyrrolidin-2-yl)methanol

: 1190971-06-2
(S)-tert-butyl 2-((1-(4-methoxy-2,6-dimethylphenylsulfonyl)pyrrolidin-2-yl)methoxy)acetate

Guidance literature:: (S)-(1-(4-methoxy-2,6-dimethylphenylsulfonyl)pyrrolidin-2-yl)methanol; With tetrabutyl-ammonium chloride; sodium hydroxide; In dichloromethane; at 20 ℃; for 0.25h;

bromoacetic acid tert-butyl ester; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 147-85-3,25191-13-3,37159-97-0,4305-67-3,4607-28-7
L-proline

: 1190971-06-2
(S)-tert-butyl 2-((1-(4-methoxy-2,6-dimethylphenylsulfonyl)pyrrolidin-2-yl)methoxy)acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Reflux

1.2: Saturated solution

2.1: triethylamine / dichloromethane / 0 - 20 °C

3.1: tetrabutyl-ammonium chloride; sodium hydroxide / dichloromethane / 0.25 h / 20 °C

3.2: 0 - 20 °C

With lithium aluminium tetrahydride; tetrabutyl-ammonium chloride; triethylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane;

Reference yield:

: 874-63-5
3,5-dimethylmethoxybenzene

: 1190971-06-2
(S)-tert-butyl 2-((1-(4-methoxy-2,6-dimethylphenylsulfonyl)pyrrolidin-2-yl)methoxy)acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: chlorosulfonic acid / dichloromethane / 0 °C

2.1: triethylamine / dichloromethane / 0 - 20 °C

3.1: tetrabutyl-ammonium chloride; sodium hydroxide / dichloromethane / 0.25 h / 20 °C

3.2: 0 - 20 °C

With chlorosulfonic acid; tetrabutyl-ammonium chloride; triethylamine; sodium hydroxide; In dichloromethane;