1-Phenylsilacyclohexane

Base Information

Chemical Name:1-Phenylsilacyclohexane
CAS No.:85125-33-3
Molecular Formula:C₁₁H₁₆Si
Molecular Weight:176.334
Hs Code.:
European Community (EC) Number:660-332-2
Nikkaji Number:J3.027.564K

Synonyms:1beta-Phenylsilacyclohexane;1-PHENYLSILACYCLOHEXANE;AKOS024338736

Suppliers and Price of 1-Phenylsilacyclohexane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1-Phenylsilacyclohexane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:1
Exact Mass:176.102127045
Heavy Atom Count:12
Complexity:121

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC[SiH](CC1)C2=CC=CC=C2

Technology Process of 1-Phenylsilacyclohexane

There total 3 articles about 1-Phenylsilacyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 18339-91-8
1-chloro-1-silacyclohexane

: 100-58-3
phenylmagnesium bromide

: 85125-33-3
1-phenyl-1-silacyclohexane

Guidance literature:: In diethyl ether; at 0 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1021/om4005725

Reference yield: 60.0%

: 29442-43-1
1‐phenyl‐1‐chloro‐1‐silacyclohexane

: 85125-33-3
1-phenyl-1-silacyclohexane

Guidance literature:: 1‐phenyl‐1‐chloro‐1‐silacyclohexane; With lithium aluminium tetrahydride; In diethyl ether; for 3h; Reflux;

With ammonium chloride; In diethyl ether; water; pentane; at 20 ℃; Saturated solution;
DOI:10.1016/j.tet.2011.10.082

Reference yield:

: 111-24-0
1,5-dibromo-pentane

: 98-13-5
Phenyltrichlorosilane

: 85125-33-3
1-phenyl-1-silacyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium

1.2: 6 h / Reflux

2.1: lithium aluminium tetrahydride / diethyl ether / 3 h / Reflux

2.2: 20 °C / Saturated solution

With lithium aluminium tetrahydride; magnesium; In diethyl ether;
DOI:10.1016/j.tet.2011.10.082