2-{5-[1-(4-Methoxy-phenyl)-meth-(Z)-ylidene]-4-oxo-4,5-dihydro-thiazol-2-yl}-acetamide

Base Information

• Chemical Name: 2-{5-[1-(4-Methoxy-phenyl)-meth-(Z)-ylidene]-4-oxo-4,5-dihydro-thiazol-2-yl}-acetamide
• CAS No.: 879197-08-7
• Molecular Formula: C₁₃H₁₂N₂O₃S
• Molecular Weight: 276.316

Synonyms:2-{5-[1-(4-Methoxy-phenyl)-meth-(Z)-ylidene]-4-oxo-4,5-dihydro-thiazol-2-yl}-acetamide

Chemical Property of 2-{5-[1-(4-Methoxy-phenyl)-meth-(Z)-ylidene]-4-oxo-4,5-dihydro-thiazol-2-yl}-acetamide

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Technology Process of 2-{5-[1-(4-Methoxy-phenyl)-meth-(Z)-ylidene]-4-oxo-4,5-dihydro-thiazol-2-yl}-acetamide

There total 1 articles about 2-{5-[1-(4-Methoxy-phenyl)-meth-(Z)-ylidene]-4-oxo-4,5-dihydro-thiazol-2-yl}-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

4-Oxo-4,5-dihydro-1,3-thiazole-2-acetamide (87947-93-1) + 4-methoxy-benzaldehyde (123-11-5) → 2-{5-[1-(4-Methoxy-phenyl)-meth-(Z)-ylidene]-4-oxo-4,5-dihydro-thiazol-2-yl}-acetamide (879197-08-7)

Guidance literature:

With piperidine; In ethanol; for 3h; Heating;

DOI:10.1080/104265090889620

Reference yield: 87.0%

2-{5-[1-(4-Methoxy-phenyl)-meth-(Z)-ylidene]-4-oxo-4,5-dihydro-thiazol-2-yl}-acetamide (879197-08-7) + 2-(4-methylbenzylidene)malononitrile (2826-25-7) → 5-amino-6-cyano-2-(4-methoxy-benzylidene)-3-oxo-7-p-tolyl-2,3-dihydro-7H-thiazolo[3,2-a]pyridine-8-carboxylic acid amide (879197-27-0)

Guidance literature:

With piperidine; In ethanol; for 6h; Heating;

DOI:10.1080/104265090889620

Reference yield: 77.0%

2-{5-[1-(4-Methoxy-phenyl)-meth-(Z)-ylidene]-4-oxo-4,5-dihydro-thiazol-2-yl}-acetamide (879197-08-7) + o-chlorobenzylidene malononitrile (2698-41-1) → 5-Amino-7-(2-chloro-phenyl)-6-cyano-2-[1-(4-methoxy-phenyl)-meth-(Z)-ylidene]-3-oxo-2,3-dihydro-7H-thiazolo[3,2-a]pyridine-8-carboxylic acid amide (879197-25-8)

Guidance literature:

With piperidine; In ethanol; for 6h; Heating;

DOI:10.1080/104265090889620

upstream raw materials:

4-Oxo-4,5-dihydro-1,3-thiazole-2-acetamide

4-methoxy-benzaldehyde

Downstream raw materials:

5-Amino-7-(2-chloro-phenyl)-6-cyano-2-[1-(4-methoxy-phenyl)-meth-(Z)-ylidene]-3-oxo-2,3-dihydro-7H-thiazolo[3,2-a]pyridine-8-carboxylic acid amide

5-amino-6-cyano-2-(4-methoxy-benzylidene)-3-oxo-7-p-tolyl-2,3-dihydro-7H-thiazolo[3,2-a]pyridine-8-carboxylic acid amide

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