N,N-diethyl O-[5-isopropoxy-4-methoxy-2-(4-isopropoxy-2-methoxyphenyl)]-1-naphthylcarbamate

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Chemical Name:N,N-diethyl O-[5-isopropoxy-4-methoxy-2-(4-isopropoxy-2-methoxyphenyl)]-1-naphthylcarbamate
CAS No.:199858-11-2
Molecular Formula:C₂₉H₃₇NO₆
Molecular Weight:495.616
Hs Code.:

Synonyms:N,N-diethyl O-[5-isopropoxy-4-methoxy-2-(4-isopropoxy-2-methoxyphenyl)]-1-naphthylcarbamate

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Chemical Property of N,N-diethyl O-[5-isopropoxy-4-methoxy-2-(4-isopropoxy-2-methoxyphenyl)]-1-naphthylcarbamate

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Technology Process of N,N-diethyl O-[5-isopropoxy-4-methoxy-2-(4-isopropoxy-2-methoxyphenyl)]-1-naphthylcarbamate

There total 4 articles about N,N-diethyl O-[5-isopropoxy-4-methoxy-2-(4-isopropoxy-2-methoxyphenyl)]-1-naphthylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 199858-09-8
4-isopropoxy-2-methoxyphenylboronic acid

: 199858-17-8
N,N-diethyl O-(2-iodo-5-isopropoxy-4-methoxy)-1-naphthylcarbamate

: 199858-11-2
N,N-diethyl O-[5-isopropoxy-4-methoxy-2-(4-isopropoxy-2-methoxyphenyl)]-1-naphthylcarbamate

Guidance literature:: With barium dihydroxide; palladium;
DOI:10.1016/S0040-4039(97)10188-5

Reference yield:

: 102127-34-4
4-bromo-3-methoxyphenol

: 199858-11-2
N,N-diethyl O-[5-isopropoxy-4-methoxy-2-(4-isopropoxy-2-methoxyphenyl)]-1-naphthylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / K₂CO₃ / acetone / Heating

2: 67 percent / 1.) n-BuLi; 3.) H₃O(+) / tetrahydrofuran / 1.) -78 deg C

3: 92 percent / Ba(OH)2 / Pd⁽⁰⁾

With barium dihydroxide; n-butyllithium; oxonium; potassium carbonate; palladium; In tetrahydrofuran; acetone;
DOI:10.1016/S0040-4039(97)10188-5

Reference yield:

: 176391-61-0
1-bromo-4-isopropoxy-2-methoxybenzene

: 199858-11-2
N,N-diethyl O-[5-isopropoxy-4-methoxy-2-(4-isopropoxy-2-methoxyphenyl)]-1-naphthylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / 1.) n-BuLi; 3.) H₃O(+) / tetrahydrofuran / 1.) -78 deg C

2: 92 percent / Ba(OH)2 / Pd⁽⁰⁾

With barium dihydroxide; n-butyllithium; oxonium; palladium; In tetrahydrofuran;
DOI:10.1016/S0040-4039(97)10188-5