C₂₃H₃₂N₂O₆

Base Information

Chemical Name:C₂₃H₃₂N₂O₆
CAS No.:1259040-31-7
Molecular Formula:C₂₃H₃₂N₂O₆
Molecular Weight:432.517
Hs Code.:

C<sub>23</sub>H<sub>32</sub>N<sub>2</sub>O<sub>6</sub>

Synonyms:C₂₃H₃₂N₂O₆

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Chemical Property of C₂₃H₃₂N₂O₆

Chemical Property:

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Technology Process of C₂₃H₃₂N₂O₆

There total 10 articles about C₂₃H₃₂N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1259040-30-6
C₂₂H₃₀N₂O₅

: 18107-18-1
diazomethyl-trimethyl-silane

: 1259040-31-7
C₂₃H₃₂N₂O₆

Guidance literature:: C₂₂H₃₀N₂O₅; With sodium hypochlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In water; tert-butyl alcohol; at 20 ℃; for 2.25h;

diazomethyl-trimethyl-silane; In methanol; hexane; for 0.0166667h;

Reference yield:

: 146603-99-8
1-(1,1-dimethylethyl) 4-ethyl 4-(2-propenyl)-1,4-piperidinedicarboxylate

: 1259040-31-7
C₂₃H₃₂N₂O₆

Guidance literature:: Multi-step reaction with 9 steps

1.1: ozone / methanol / 1 h / -78 °C

1.2: 15 h / 20 °C

2.1: acetic acid; sodium tris(acetoxy)borohydride / N,N-dimethyl-formamide / 21 h / 20 - 40 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / tetrahydrofuran / 2 h / -40 °C / Inert atmosphere

3.2: 0.5 h / -40 - 20 °C

4.1: lithium diisopropyl amide; N,N,N,N,N,N-hexamethylphosphoric triamide / n-heptane; tetrahydrofuran; ethylbenzene / 0.08 h / -78 °C / Inert atmosphere

4.2: 1.5 h

5.1: water; sodium tetrahydroborate / ethanol / 5 h / 20 °C

6.1: hydrogen / 10 wt% Pd(OH)2 on carbon / ethanol / 3 h / 60 °C

7.1: sodium carbonate / tetrahydrofuran / 3 h

8.1: triethanolamine; pyridine-SO₃ complex; dimethyl sulfoxide / dichloromethane / 24 h / 0 - 20 °C / Inert atmosphere

9.1: 2-methyl-but-2-ene; sodium hypochlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol / 2.25 h / 20 °C

9.2: 0.02 h

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hypochlorite; sodium tetrahydroborate; sodium dihydrogenphosphate; 2-methyl-but-2-ene; pyridine-SO₃ complex; triethanolamine; water; hydrogen; sodium tris(acetoxy)borohydride; diisobutylaluminium hydride; sodium carbonate; ozone; acetic acid; dimethyl sulfoxide; lithium diisopropyl amide; 10 wt% Pd(OH)2 on carbon; In tetrahydrofuran; methanol; ethanol; n-heptane; dichloromethane; ethylbenzene; water; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

: C₂₃H₃₄N₂O₄

: 1259040-31-7
C₂₃H₃₂N₂O₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: water; sodium tetrahydroborate / ethanol / 5 h / 20 °C

2.1: hydrogen / 10 wt% Pd(OH)2 on carbon / ethanol / 3 h / 60 °C

3.1: sodium carbonate / tetrahydrofuran / 3 h

4.1: triethanolamine; pyridine-SO₃ complex; dimethyl sulfoxide / dichloromethane / 24 h / 0 - 20 °C / Inert atmosphere

5.1: 2-methyl-but-2-ene; sodium hypochlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol / 2.25 h / 20 °C

5.2: 0.02 h

With sodium hypochlorite; sodium tetrahydroborate; sodium dihydrogenphosphate; 2-methyl-but-2-ene; pyridine-SO₃ complex; triethanolamine; water; hydrogen; sodium carbonate; dimethyl sulfoxide; 10 wt% Pd(OH)2 on carbon; In tetrahydrofuran; ethanol; dichloromethane; water; tert-butyl alcohol;