D-6-benzyloxycarbonylamino-6-carbamoylhexanoyl-D-alanyl-D-alanine benzyl ester

Base Information

Chemical Name:D-6-benzyloxycarbonylamino-6-carbamoylhexanoyl-D-alanyl-D-alanine benzyl ester
CAS No.:1429301-64-3
Molecular Formula:C₂₈H₃₆N₄O₇
Molecular Weight:540.616
Hs Code.:

Synonyms:D-6-benzyloxycarbonylamino-6-carbamoylhexanoyl-D-alanyl-D-alanine benzyl ester

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Chemical Property of D-6-benzyloxycarbonylamino-6-carbamoylhexanoyl-D-alanyl-D-alanine benzyl ester

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Technology Process of D-6-benzyloxycarbonylamino-6-carbamoylhexanoyl-D-alanyl-D-alanine benzyl ester

There total 7 articles about D-6-benzyloxycarbonylamino-6-carbamoylhexanoyl-D-alanyl-D-alanine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1429301-63-2
D-6-benzyloxycarbonylamino-6-[N-(2',4'-dimethoxybenzyl)carbamoyl]hexanoyl-D-alanyl-D-alanine benzyl ester

: 1429301-64-3
D-6-benzyloxycarbonylamino-6-carbamoylhexanoyl-D-alanyl-D-alanine benzyl ester

Guidance literature:: With trifluoroacetic acid; at 20 ℃; for 3.5h;
DOI:10.1021/bi400211q

Reference yield:

: 1429301-61-0
D-6-benzyloxycarbonylamino-6-[N-(2′,4′-dimethoxybenzyl)carbamoyl]hexanoic acid ethyl ester

: 1429301-64-3
D-6-benzyloxycarbonylamino-6-carbamoylhexanoyl-D-alanyl-D-alanine benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: lithium hydroxide / tetrahydrofuran; water / 5 - 10 °C

2: 1-hydroxy-pyrrolidine-2,5-dione; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide / N,N-dimethyl-formamide / 20 h / 20 °C

3: trifluoroacetic acid / 3.5 h / 20 °C

With 1-hydroxy-pyrrolidine-2,5-dione; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; trifluoroacetic acid; lithium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1021/bi400211q

Reference yield:

: 1429301-62-1
D-6-benzyloxycarbonylamino-6-[N-(2′,4′-dimethoxybenzyl)carbamoyl]hexanoic acid

: 1429301-64-3
D-6-benzyloxycarbonylamino-6-carbamoylhexanoyl-D-alanyl-D-alanine benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1-hydroxy-pyrrolidine-2,5-dione; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide / N,N-dimethyl-formamide / 20 h / 20 °C

2: trifluoroacetic acid / 3.5 h / 20 °C

With 1-hydroxy-pyrrolidine-2,5-dione; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1021/bi400211q