(2Z)-ethyl 2-(4-(2-chlorophenyl)-3,3-dicyano-2-(2,6-dimethylphenylimino)cyclopentylidene)propanoate

Base Information

Chemical Name:(2Z)-ethyl 2-(4-(2-chlorophenyl)-3,3-dicyano-2-(2,6-dimethylphenylimino)cyclopentylidene)propanoate
CAS No.:1308874-58-9
Molecular Formula:C₂₆H₂₄ClN₃O₂
Molecular Weight:445.948
Hs Code.:

Synonyms:(2Z)-ethyl 2-(4-(2-chlorophenyl)-3,3-dicyano-2-(2,6-dimethylphenylimino)cyclopentylidene)propanoate

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Chemical Property of (2Z)-ethyl 2-(4-(2-chlorophenyl)-3,3-dicyano-2-(2,6-dimethylphenylimino)cyclopentylidene)propanoate

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Technology Process of (2Z)-ethyl 2-(4-(2-chlorophenyl)-3,3-dicyano-2-(2,6-dimethylphenylimino)cyclopentylidene)propanoate

There total 5 articles about (2Z)-ethyl 2-(4-(2-chlorophenyl)-3,3-dicyano-2-(2,6-dimethylphenylimino)cyclopentylidene)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 2698-41-1
o-chlorobenzylidene malononitrile

: 5717-41-9
ethyl 2-methylbuta-2,3-dienoate

: 119072-54-7,2769-71-3
2,6-dimethylphenyl isonitrile

: 1308874-58-9
(2Z)-ethyl 2-(4-(2-chlorophenyl)-3,3-dicyano-2-(2,6-dimethylphenylimino)cyclopentylidene)propanoate

Guidance literature:: With silver hexafluoroantimonate; In toluene; at 120 ℃; for 24h; stereoselective reaction;
DOI:10.1002/adsc.201000795

Reference yield:

: 30018-16-7
(1-ethoxycarbonylethyl)triphenylphosphonium bromide

: 1308874-58-9
(2Z)-ethyl 2-(4-(2-chlorophenyl)-3,3-dicyano-2-(2,6-dimethylphenylimino)cyclopentylidene)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / hexane; dichloromethane / 2 h / 0 °C

1.2: 0 °C

2.1: silver hexafluoroantimonate / toluene / 24 h / 120 °C

With silver hexafluoroantimonate; triethylamine; In hexane; dichloromethane; toluene;
DOI:10.1002/adsc.201000795

Reference yield:

: 607-92-1
2,6-dimethylformanilide

: 1308874-58-9
(2Z)-ethyl 2-(4-(2-chlorophenyl)-3,3-dicyano-2-(2,6-dimethylphenylimino)cyclopentylidene)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; trichlorophosphate / dichloromethane / 0 °C

1.2: 1 h / 20 - 30 °C

2.1: silver hexafluoroantimonate / toluene / 24 h / 120 °C

With silver hexafluoroantimonate; triethylamine; trichlorophosphate; In dichloromethane; toluene;
DOI:10.1002/adsc.201000795