1,3,5-tris<(S)-1-(1-O-benzyl-β-alaninyl)-3-(4-biphenylyl)-1-oxo-2-propyl>hexahydro-1,3,5-triazine

Base Information

Chemical Name:1,3,5-tris<(S)-1-(1-O-benzyl-β-alaninyl)-3-(4-biphenylyl)-1-oxo-2-propyl>hexahydro-1,3,5-triazine
CAS No.:147862-25-7
Molecular Formula:C₇₈H₇₈N₆O₉
Molecular Weight:1243.51
Hs Code.:

Synonyms:1,3,5-tris<(S)-1-(1-O-benzyl-β-alaninyl)-3-(4-biphenylyl)-1-oxo-2-propyl>hexahydro-1,3,5-triazine

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Chemical Property of 1,3,5-tris<(S)-1-(1-O-benzyl-β-alaninyl)-3-(4-biphenylyl)-1-oxo-2-propyl>hexahydro-1,3,5-triazine

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Technology Process of 1,3,5-tris<(S)-1-(1-O-benzyl-β-alaninyl)-3-(4-biphenylyl)-1-oxo-2-propyl>hexahydro-1,3,5-triazine

There total 1 articles about 1,3,5-tris<(S)-1-(1-O-benzyl-β-alaninyl)-3-(4-biphenylyl)-1-oxo-2-propyl>hexahydro-1,3,5-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: (S)-(4-phenylphenylalanyl)-β-alanine benzyl ester hydrochloride

: 147862-25-7
1,3,5-tris<(S)-1-(1-O-benzyl-β-alaninyl)-3-(4-biphenylyl)-1-oxo-2-propyl>hexahydro-1,3,5-triazine

Guidance literature:: With sodium hydrogencarbonate; In water; ethyl acetate; a) 0 deg C, 1 h, b) RT, 18 h;

Reference yield: 90.7%

: 4712-55-4
diphenyl hydrogen phosphite

: 147862-25-7
1,3,5-tris<(S)-1-(1-O-benzyl-β-alaninyl)-3-(4-biphenylyl)-1-oxo-2-propyl>hexahydro-1,3,5-triazine

: 147862-02-0
benzyl (S)-N-[2-(diphenylphosphonomethylamino)-3-(4-biphenylyl)-propionyl]-3-aminopropionate

Guidance literature:: In toluene; at 70 ℃; for 1.25h;

Reference yield:

: 147862-25-7
1,3,5-tris<(S)-1-(1-O-benzyl-β-alaninyl)-3-(4-biphenylyl)-1-oxo-2-propyl>hexahydro-1,3,5-triazine

: 147862-05-3
N,N-diethylcarbamoylmethyl (S)-N-[2-(diphenylphosphonomethylamino)-3-(4-biphenylyl)-propionyl]-3-aminopropionate

Guidance literature:: Multi-step reaction with 3 steps

1: 90.7 percent / toluene / 1.25 h / 70 °C

2: 67 percent / H₂ / 10percent Pd/C / ethyl acetate / 5.5 h / 2585.7 Torr

3: 68 percent / Et₃N, NaI / ethyl acetate / 12 h / 80 °C

With hydrogen; triethylamine; sodium iodide; palladium on activated charcoal; In ethyl acetate; toluene;