methyl (2E)-2-{[N-(2-formylphenyl)(4-methylbenzene)sulfonamido] methyl}-3-(2-methoxyphenyl)prop-2-enoate

Base Information

• Chemical Name: methyl (2E)-2-{[N-(2-formylphenyl)(4-methylbenzene)sulfonamido] methyl}-3-(2-methoxyphenyl)prop-2-enoate
• CAS No.: 1589493-39-9
• Molecular Formula: C₂₆H₂₅NO₆S
• Molecular Weight: 479.554

Synonyms:methyl (2E)-2-{[N-(2-formylphenyl)(4-methylbenzene)sulfonamido] methyl}-3-(2-methoxyphenyl)prop-2-enoate

Chemical Property of methyl (2E)-2-{[N-(2-formylphenyl)(4-methylbenzene)sulfonamido] methyl}-3-(2-methoxyphenyl)prop-2-enoate

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Technology Process of methyl (2E)-2-{[N-(2-formylphenyl)(4-methylbenzene)sulfonamido] methyl}-3-(2-methoxyphenyl)prop-2-enoate

There total 6 articles about methyl (2E)-2-{[N-(2-formylphenyl)(4-methylbenzene)sulfonamido] methyl}-3-(2-methoxyphenyl)prop-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

N-(2-Formyl-phenyl)-4-methyl-benzenesulfonamide (6590-65-4) + (Z)-methyl 2-(bromomethyl)-3-(2-methoxyphenyl)acrylate → methyl (2E)-2-{[N-(2-formylphenyl)(4-methylbenzene)sulfonamido] methyl}-3-(2-methoxyphenyl)prop-2-enoate (1589493-39-9)

Guidance literature:

N-(2-Formyl-phenyl)-4-methyl-benzenesulfonamide; With potassium carbonate; In acetonitrile; at 20 ℃; for 0.25h;

(Z)-methyl 2-(bromomethyl)-3-(2-methoxyphenyl)acrylate; In acetonitrile; for 2h;

DOI:10.1016/j.molstruc.2016.08.001

Reference yield: 97.0%

(Z)-2-Bromomethyl-3-(2-methoxy-phenyl)-acrylic acid methyl ester (139413-77-7) + N-(2-Formyl-phenyl)-4-methyl-benzenesulfonamide (6590-65-4) → methyl (2E)-2-{[N-(2-formylphenyl)(4-methylbenzene)sulfonamido] methyl}-3-(2-methoxyphenyl)prop-2-enoate (1589493-39-9)

Guidance literature:

N-(2-Formyl-phenyl)-4-methyl-benzenesulfonamide; With potassium carbonate; In acetonitrile; at 20 ℃; for 0.25h;

(Z)-2-Bromomethyl-3-(2-methoxy-phenyl)-acrylic acid methyl ester; In acetonitrile; at 20 ℃; for 3h;

DOI:10.1039/c5ob01060h

Reference yield:

N-(2-hydroxymethylphenyl)-4-methylbenzenesulfonamide (90312-02-0) → methyl (2E)-2-{[N-(2-formylphenyl)(4-methylbenzene)sulfonamido] methyl}-3-(2-methoxyphenyl)prop-2-enoate (1589493-39-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: manganese(IV) oxide

2.1: potassium carbonate / acetonitrile / 0.25 h / 20 °C

2.2: 3 h / 20 °C

With manganese(IV) oxide; potassium carbonate; In acetonitrile;

DOI:10.1039/c5ob01060h

upstream raw materials:

(Z)-2-Bromomethyl-3-(2-methoxy-phenyl)-acrylic acid methyl ester

N-(2-Formyl-phenyl)-4-methyl-benzenesulfonamide

methyl 2-(hydroxy(2-methoxyphenyl)methyl)acrylate

N-(2-hydroxymethylphenyl)-4-methylbenzenesulfonamide

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