C₂₂H₂₆N₂O₄

Base Information

Chemical Name:C₂₂H₂₆N₂O₄
CAS No.:1344689-16-2
Molecular Formula:C₂₂H₂₆N₂O₄
Molecular Weight:382.459
Hs Code.:

C<sub>22</sub>H<sub>26</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C₂₂H₂₆N₂O₄

Suppliers and Price of C₂₂H₂₆N₂O₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₂H₂₆N₂O₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₂H₂₆N₂O₄

There total 10 articles about C₂₂H₂₆N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₂H₄₂N₂O₇

: 1344689-16-2
C₂₂H₂₆N₂O₄

Guidance literature:: With water; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 6h;

Reference yield:

: 93-17-4
3,4-dimethoxyphenylacetonitrile

: 1344689-16-2
C₂₂H₂₆N₂O₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium / ethanol; toluene

1.2: 80 °C

2.1: hydrogenchloride; palladium on activated charcoal; hydrogen / ethanol / 2585.81 Torr

3.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / dichloromethane

4.1: phosphorus pentachloride / dichloromethane

5.1: sulfur / 165 °C / neat (no solvent)

6.1: lithium aluminium tetrahydride / tetrahydrofuran

7.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran

8.1: trifluoroacetic acid / dichloromethane

With hydrogenchloride; lithium aluminium tetrahydride; phosphorus pentachloride; palladium on activated charcoal; hydrogen; sodium; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; sulfur; triethylamine; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In tetrahydrofuran; ethanol; dichloromethane; toluene; 4.1: Bischler-Napieralski reaction;
DOI:10.1016/j.bmcl.2011.09.009

Reference yield:

: 36848-69-8
ethyl 2-cyano-2-(3,4-dimethoxyphenyl)acetate

: 1344689-16-2
C₂₂H₂₆N₂O₄

Guidance literature:: Multi-step reaction with 7 steps

1: hydrogenchloride; palladium on activated charcoal; hydrogen / ethanol / 2585.81 Torr

2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / dichloromethane

3: phosphorus pentachloride / dichloromethane

4: sulfur / 165 °C / neat (no solvent)

5: lithium aluminium tetrahydride / tetrahydrofuran

6: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran

7: trifluoroacetic acid / dichloromethane

With hydrogenchloride; lithium aluminium tetrahydride; phosphorus pentachloride; palladium on activated charcoal; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; sulfur; triethylamine; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In tetrahydrofuran; ethanol; dichloromethane; 3: Bischler-Napieralski reaction;
DOI:10.1016/j.bmcl.2011.09.009