methyl 3-{4-[2-acetoxy-2-(5-ethyl-2-pyridyl) ethoxy]phenyl}-2-bromopropionate

Base Information

Chemical Name:methyl 3-{4-[2-acetoxy-2-(5-ethyl-2-pyridyl) ethoxy]phenyl}-2-bromopropionate
CAS No.:101931-09-3
Molecular Formula:C₂₁H₂₄BrNO₅
Molecular Weight:450.329
Hs Code.:

Synonyms:methyl 3-{4-[2-acetoxy-2-(5-ethyl-2-pyridyl) ethoxy]phenyl}-2-bromopropionate

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Chemical Property of methyl 3-{4-[2-acetoxy-2-(5-ethyl-2-pyridyl) ethoxy]phenyl}-2-bromopropionate

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Technology Process of methyl 3-{4-[2-acetoxy-2-(5-ethyl-2-pyridyl) ethoxy]phenyl}-2-bromopropionate

There total 7 articles about methyl 3-{4-[2-acetoxy-2-(5-ethyl-2-pyridyl) ethoxy]phenyl}-2-bromopropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85583-40-0
4-[2-(5-ethylpyridin-2-yl)ethoxy]aniline

: 101931-09-3
methyl 3-{4-[2-acetoxy-2-(5-ethyl-2-pyridyl) ethoxy]phenyl}-2-bromopropionate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.)47percent HBr, NaNO₂, 2.)Cu₂O / 1.)MeOH, H₂O, 5 deg C, 20 min., 2.)40 deg C

2: 70percent m-chloroperbenzoic acid / methanol / Heating

3: 80 °C

With copper(I) oxide; hydrogen bromide; 3-chloro-benzenecarboperoxoic acid; sodium nitrite; In methanol;

Reference yield:

: 5223-06-3
5-ethyl-2-(2-hydroxyethyl)pyridine

: 101931-09-3
methyl 3-{4-[2-acetoxy-2-(5-ethyl-2-pyridyl) ethoxy]phenyl}-2-bromopropionate

Guidance literature:: Multi-step reaction with 5 steps

1: 63 percent / NaH / dimethylformamide

2: H₂ / 10percent Pd-C / methanol / 760 Torr / Ambient temperature

3: 1.)47percent HBr, NaNO₂, 2.)Cu₂O / 1.)MeOH, H₂O, 5 deg C, 20 min., 2.)40 deg C

4: 70percent m-chloroperbenzoic acid / methanol / Heating

5: 80 °C

With copper(I) oxide; hydrogen bromide; hydrogen; sodium hydride; 3-chloro-benzenecarboperoxoic acid; sodium nitrite; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 85583-54-6
4-[2-(5-ethyl-2-pyridyl)ethoxy]nitrobenzene

: 101931-09-3
methyl 3-{4-[2-acetoxy-2-(5-ethyl-2-pyridyl) ethoxy]phenyl}-2-bromopropionate

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / 10percent Pd-C / methanol / 760 Torr / Ambient temperature

2: 1.)47percent HBr, NaNO₂, 2.)Cu₂O / 1.)MeOH, H₂O, 5 deg C, 20 min., 2.)40 deg C

3: 70percent m-chloroperbenzoic acid / methanol / Heating

4: 80 °C

With copper(I) oxide; hydrogen bromide; hydrogen; 3-chloro-benzenecarboperoxoic acid; sodium nitrite; palladium on activated charcoal; In methanol;