C₃₃H₃₁IN₂O₇

Base Information

Chemical Name:C₃₃H₃₁IN₂O₇
CAS No.:957785-29-4
Molecular Formula:C₃₃H₃₁IN₂O₇
Molecular Weight:694.523
Hs Code.:

C<sub>33</sub>H<sub>31</sub>IN<sub>2</sub>O<sub>7</sub>

Synonyms:C₃₃H₃₁IN₂O₇

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Chemical Property of C₃₃H₃₁IN₂O₇

Chemical Property:

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Technology Process of C₃₃H₃₁IN₂O₇

There total 11 articles about C₃₃H₃₁IN₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 957785-28-3
3-methyl-4-[(3,4-dimethoxy-2-phenylmethoxy)phenyl]-6-[(5,6,8-trimethoxy)-2-quinolinyl]-(1H)-2-pyridinone

: 957785-29-4
C₃₃H₃₁IN₂O₇

Guidance literature:: With Iodine monochloride; potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1021/jo701435p

Reference yield:

: 957785-13-6
4-chloro-5,6,8-trimethoxyquinoline-2-carboxylic acid methyl ester

: 957785-29-4
C₃₃H₃₁IN₂O₇

Guidance literature:: Multi-step reaction with 5 steps

1.1: 100 percent / hydrogen; Et₃N / Pd-C / ethyl acetate / 0.75 h / 20 °C

2.1: NaH / toluene / 15 h / 110 °C

2.2: 78 percent / aq. HCl / dioxane / 15 h / 70 °C

3.1: 83 percent / NaOH / ethanol; H₂O / 15 h / 20 °C

4.1: 60 percent / potassium tert-butoxide / dimethylsulfoxide / 5 h / 100 °C

5.1: potassium carbonate; iodine monochloride / dimethylformamide / 16 h / 20 °C

With sodium hydroxide; potassium tert-butylate; hydrogen; Iodine monochloride; sodium hydride; potassium carbonate; triethylamine; palladium on activated charcoal; In ethanol; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo701435p

Reference yield:

: 2-[(2,4,5-trimethoxyphenyl)amino]-2-butenedioic acid dimethyl ester

: 957785-29-4
C₃₃H₃₁IN₂O₇

Guidance literature:: Multi-step reaction with 7 steps

1.1: 86 percent / diphenyl ether / 2 h / Heating

2.1: 88 percent / POCl₃ / benzene / 24 h / 20 °C

3.1: 100 percent / hydrogen; Et₃N / Pd-C / ethyl acetate / 0.75 h / 20 °C

4.1: NaH / toluene / 15 h / 110 °C

4.2: 78 percent / aq. HCl / dioxane / 15 h / 70 °C

5.1: 83 percent / NaOH / ethanol; H₂O / 15 h / 20 °C

6.1: 60 percent / potassium tert-butoxide / dimethylsulfoxide / 5 h / 100 °C

7.1: potassium carbonate; iodine monochloride / dimethylformamide / 16 h / 20 °C

With sodium hydroxide; potassium tert-butylate; hydrogen; Iodine monochloride; sodium hydride; potassium carbonate; triethylamine; trichlorophosphate; palladium on activated charcoal; In diphenylether; ethanol; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; toluene; benzene;
DOI:10.1021/jo701435p