Technology Process of
There total 8 articles about which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
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In
solid;
byproducts: H2O; High Pressure; synthesized by intense high-pressure shear treatment (Usp. Khim., 2001, vol. 70, no. 1, pp. 72-87);
DOI:10.1023/B:RJAC.0000038827.10443.63
- Guidance literature:
-
In
water;
High Pressure; placed in a bomb, heated to 220°C (3 h), held for 3 h; cooled to room temp. (3 h), crysts., washed (methanol), dried (desiccator, 24 h); elem. anal.;
DOI:10.1016/S0277-5387(03)00461-3
- Guidance literature:
-
In
neat (no solvent);
byproducts: CH3COOH; stoich. mixt. stirred at 180°C (thermotstated oil reactor) for 3 h; CH3COOH stripped by N2 stream, collected in condensor;
DOI:10.1016/j.molcata.2005.05.041
