2-[6-(3,5-dimethoxyphenyl)-2,3-dihydrobenzo[1,2-b;5,4-b']difuran-2-yl]propan-2-ol

Base Information

Chemical Name:2-[6-(3,5-dimethoxyphenyl)-2,3-dihydrobenzo[1,2-b;5,4-b']difuran-2-yl]propan-2-ol
CAS No.:1310328-29-0
Molecular Formula:C₂₁H₂₂O₅
Molecular Weight:354.403
Hs Code.:

Synonyms:2-[6-(3,5-dimethoxyphenyl)-2,3-dihydrobenzo[1,2-b;5,4-b']difuran-2-yl]propan-2-ol

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Chemical Property of 2-[6-(3,5-dimethoxyphenyl)-2,3-dihydrobenzo[1,2-b;5,4-b']difuran-2-yl]propan-2-ol

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Technology Process of 2-[6-(3,5-dimethoxyphenyl)-2,3-dihydrobenzo[1,2-b;5,4-b']difuran-2-yl]propan-2-ol

There total 8 articles about 2-[6-(3,5-dimethoxyphenyl)-2,3-dihydrobenzo[1,2-b;5,4-b']difuran-2-yl]propan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.8%

: 1155310-14-7
2-(1-hydroxy-1-methyl-ethyl)-5-iodo-2,3-dihydro-benzofuran-6-ol

: 171290-52-1
1-Ethynyl-3,5-dimethoxy-benzene

: 1310328-29-0
2-[6-(3,5-dimethoxyphenyl)-2,3-dihydrobenzo[1,2-b;5,4-b']difuran-2-yl]propan-2-ol

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In 1,4-dioxane; at 85 ℃; for 20h; Inert atmosphere;
DOI:10.1016/j.ejmech.2011.03.022

Reference yield:

: 4806-05-7
2-(1-hydroxy-1-methylethyl)-2,3-dihydrobenzofuran-6-ol

: 1310328-29-0
2-[6-(3,5-dimethoxyphenyl)-2,3-dihydrobenzo[1,2-b;5,4-b']difuran-2-yl]propan-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: Iodine monochloride; acetic acid / 3 h

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 1,4-dioxane / 20 h / 85 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; Iodine monochloride; acetic acid; triethylamine; In 1,4-dioxane;
DOI:10.1016/j.ejmech.2011.03.022

Reference yield:

: 205746-51-6
3,5-dimethoxy-β,β-dibromostyrene

: 1310328-29-0
2-[6-(3,5-dimethoxyphenyl)-2,3-dihydrobenzo[1,2-b;5,4-b']difuran-2-yl]propan-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: lithium diisopropyl amide / tetrahydrofuran; n-heptane; ethylbenzene / 2 h / -78 °C

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 1,4-dioxane / 20 h / 85 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane; n-heptane; ethylbenzene;
DOI:10.1016/j.ejmech.2011.03.022