(S)-4-(4-aminophenyl)-3-tert-butoxycarbonylaminobutyric acid 2-trimethylsilanyl ethyl ester

Base Information

Chemical Name:(S)-4-(4-aminophenyl)-3-tert-butoxycarbonylaminobutyric acid 2-trimethylsilanyl ethyl ester
CAS No.:151291-14-4
Molecular Formula:C₂₀H₃₄N₂O₄Si
Molecular Weight:394.586
Hs Code.:

Synonyms:(S)-4-(4-aminophenyl)-3-tert-butoxycarbonylaminobutyric acid 2-trimethylsilanyl ethyl ester

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Chemical Property of (S)-4-(4-aminophenyl)-3-tert-butoxycarbonylaminobutyric acid 2-trimethylsilanyl ethyl ester

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Technology Process of (S)-4-(4-aminophenyl)-3-tert-butoxycarbonylaminobutyric acid 2-trimethylsilanyl ethyl ester

There total 5 articles about (S)-4-(4-aminophenyl)-3-tert-butoxycarbonylaminobutyric acid 2-trimethylsilanyl ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 151291-13-3
(S)-3-tert-butoxycarbonylamino-4-(4-nitrophenyl)butyric acid 2-trimethylsilanyl ethyl ester

: 151291-14-4
(S)-4-(4-aminophenyl)-3-tert-butoxycarbonylaminobutyric acid 2-trimethylsilanyl ethyl ester

Guidance literature:: With hydrogen; palladium dihydroxide; In ethanol; under 2585.7 Torr;
DOI:10.1016/0968-0896(96)00185-X

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 151291-14-4
(S)-4-(4-aminophenyl)-3-tert-butoxycarbonylaminobutyric acid 2-trimethylsilanyl ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: aq. NaOH, NaHCO₃ / dioxane / 0 - 20 °C

2: N-methyl morpholine / tetrahydrofuran

3: diethyl ether / 0 - 20 °C

4: silver benzoate, Et₃N

5: 61 percent / H₂ / Pd(OH)2 / ethanol / 2585.7 Torr

With 4-methyl-morpholine; sodium hydroxide; hydrogen; silver benzoate; sodium hydrogencarbonate; triethylamine; palladium dihydroxide; In tetrahydrofuran; 1,4-dioxane; diethyl ether; ethanol;
DOI:10.1016/0968-0896(96)00185-X

Reference yield:

: 949-99-5
4-nitro-3-phenyl-L-alanine

: 151291-14-4
(S)-4-(4-aminophenyl)-3-tert-butoxycarbonylaminobutyric acid 2-trimethylsilanyl ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: aq. NaOH, NaHCO₃ / dioxane / 0 - 20 °C

2: N-methyl morpholine / tetrahydrofuran

3: diethyl ether / 0 - 20 °C

4: silver benzoate, Et₃N

5: 61 percent / H₂ / Pd(OH)2 / ethanol / 2585.7 Torr

With 4-methyl-morpholine; sodium hydroxide; hydrogen; silver benzoate; sodium hydrogencarbonate; triethylamine; palladium dihydroxide; In tetrahydrofuran; 1,4-dioxane; diethyl ether; ethanol;
DOI:10.1016/0968-0896(96)00185-X