(S)-(-)-N-trifluoroacetyl-2,3,6,7-tetrahydro-4-alanylbenzo[1,2-b;4,5-b']difuran

Base Information

Chemical Name:(S)-(-)-N-trifluoroacetyl-2,3,6,7-tetrahydro-4-alanylbenzo[1,2-b;4,5-b']difuran
CAS No.:332012-03-0
Molecular Formula:C₁₅H₁₄F₃NO₄
Molecular Weight:329.276
Hs Code.:

Synonyms:(S)-(-)-N-trifluoroacetyl-2,3,6,7-tetrahydro-4-alanylbenzo[1,2-b;4,5-b']difuran

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-(-)-N-trifluoroacetyl-2,3,6,7-tetrahydro-4-alanylbenzo[1,2-b;4,5-b']difuran

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Technology Process of (S)-(-)-N-trifluoroacetyl-2,3,6,7-tetrahydro-4-alanylbenzo[1,2-b;4,5-b']difuran

There total 1 articles about (S)-(-)-N-trifluoroacetyl-2,3,6,7-tetrahydro-4-alanylbenzo[1,2-b;4,5-b']difuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81926-24-1
4,10-dioxatricyclo[7.3.0.0^3,7]dodeca-1,3⁽⁷⁾,8-triene

: 56271-78-4
(S)-N-trifluoroacetyl-L-alanyl chloride

: 332012-03-0
(S)-(-)-N-trifluoroacetyl-2,3,6,7-tetrahydro-4-alanylbenzo[1,2-b;4,5-b']difuran

Guidance literature:: With aluminium trichloride; In dichloromethane; for 16h;
DOI:10.1021/jm000491y

Reference yield:

: 332012-03-0
(S)-(-)-N-trifluoroacetyl-2,3,6,7-tetrahydro-4-alanylbenzo[1,2-b;4,5-b']difuran

: 219986-75-1
(S)-(+)-1-(8-bromo-2,3,6,7-tetrahydrobenzo[1,2-b;4,5-b']difuran-4-yl)-2-aminopropane

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / TFA; Et₃SiH / 6 h / Heating

2: 82 percent / Br₂ / acetic acid / 4.5 h / 20 °C

3: aq. 5 N NaOH / methanol

With triethylsilane; sodium hydroxide; bromine; trifluoroacetic acid; In methanol; acetic acid;
DOI:10.1021/jm000491y