C₉H⁽²⁾H₁₁

Base Information

• Chemical Name: C₉H⁽²⁾H₁₁
• CAS No.: 97732-77-9
• Molecular Formula: C₉H₁₂
• Molecular Weight: 131.107
• Mol file: 97732-77-9.mol

Synonyms:C₉H⁽²⁾H₁₁

Chemical Property of C₉H⁽²⁾H₁₁

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₉H⁽²⁾H₁₁

There total 3 articles about C₉H⁽²⁾H₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1,1,3,3,3-hexadeuterio-2-bromopropane (52809-76-4) + bromobenzene-d5 (4165-57-5) → C9H(2)H11 (97732-77-9)

Guidance literature:

bromobenzene-d5; With magnesium; In tetrahydrofuran; hexane; chloroform; at 200 ℃; for 1h; under 37503.8 Torr;

1,1,1,3,3,3-hexadeuterio-2-bromopropane; With iodine; In tetrahydrofuran; hexane; chlorobenzene; at -20 ℃; for 18h;

Reference yield:

Isopropylbenzene (98-82-8) → C9H(2)H11 (97732-77-9)

Guidance literature:

With trifluoroacetic acid-d₁; [Rh(bdmpza)Cl₃](-)Na(+); silver trifluoromethanesulfonate; at 100 ℃; for 24h; Inert atmosphere;

DOI:10.1021/om2012419

Reference yield:

benzene-d6 (1076-43-3) → C9H(2)H11 (97732-77-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; ferric(III) bromide / acetonitrile / 7 h / 90 °C

2.1: magnesium / tetrahydrofuran; chloroform; hexane / 1 h / 200 °C / 37503.8 Torr

2.2: 18 h / -20 °C

With ferric(III) bromide; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; magnesium; In tetrahydrofuran; hexane; chloroform; acetonitrile;

upstream raw materials:

Isopropylbenzene

1,1,1,3,3,3-hexadeuterio-2-bromopropane

bromobenzene-d5

benzene-d6