Technology Process of methyl 4-methoxy-3,5-dimethylphloroglucinol carboxylate
There total 7 articles about methyl 4-methoxy-3,5-dimethylphloroglucinol carboxylate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
methanol; chloroform;
at 20 ℃;
for 10h;
DOI:10.1002/anie.202104014
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / acetone / 10 h / 45 °C / Inert atmosphere
1.2: 0 - 20 °C / Inert atmosphere
2.1: palladium 10% on activated carbon; hydrogen / methanol; chloroform / 6.5 h / 20 °C
3.1: titanium tetrachloride / dichloromethane / 3 h / -40 - 20 °C / Inert atmosphere
4.1: palladium 10% on activated carbon; hydrogen / methanol; chloroform / 10 h / 20 °C
With
palladium 10% on activated carbon; hydrogen; titanium tetrachloride; potassium carbonate;
In
methanol; dichloromethane; chloroform; acetone;
DOI:10.1002/anie.202104014
- Guidance literature:
-
Multi-step reaction with 3 steps
1: palladium 10% on activated carbon; hydrogen / methanol; chloroform / 6.5 h / 20 °C
2: titanium tetrachloride / dichloromethane / 3 h / -40 - 20 °C / Inert atmosphere
3: palladium 10% on activated carbon; hydrogen / methanol; chloroform / 10 h / 20 °C
With
palladium 10% on activated carbon; hydrogen; titanium tetrachloride;
In
methanol; dichloromethane; chloroform;
DOI:10.1002/anie.202104014
