(S)-(-)-N-trifluoroacetyl-1-(2,3,6,7-tetrahydrobenzo[1,2-b;4,5-b']difuran-4-yl)-2-aminopropane

Base Information

Chemical Name:(S)-(-)-N-trifluoroacetyl-1-(2,3,6,7-tetrahydrobenzo[1,2-b;4,5-b']difuran-4-yl)-2-aminopropane
CAS No.:332012-05-2
Molecular Formula:C₁₅H₁₆F₃NO₃
Molecular Weight:315.292
Hs Code.:

Synonyms:(S)-(-)-N-trifluoroacetyl-1-(2,3,6,7-tetrahydrobenzo[1,2-b;4,5-b']difuran-4-yl)-2-aminopropane

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Chemical Property of (S)-(-)-N-trifluoroacetyl-1-(2,3,6,7-tetrahydrobenzo[1,2-b;4,5-b']difuran-4-yl)-2-aminopropane

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Technology Process of (S)-(-)-N-trifluoroacetyl-1-(2,3,6,7-tetrahydrobenzo[1,2-b;4,5-b']difuran-4-yl)-2-aminopropane

There total 1 articles about (S)-(-)-N-trifluoroacetyl-1-(2,3,6,7-tetrahydrobenzo[1,2-b;4,5-b']difuran-4-yl)-2-aminopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81926-24-1
4,10-dioxatricyclo[7.3.0.0^3,7]dodeca-1,3⁽⁷⁾,8-triene

: 332012-05-2
(S)-(-)-N-trifluoroacetyl-1-(2,3,6,7-tetrahydrobenzo[1,2-b;4,5-b']difuran-4-yl)-2-aminopropane

Guidance literature:: Multi-step reaction with 2 steps

1: AlCl₃ / CH₂Cl₂ / 16 h

2: 94 percent / TFA; Et₃SiH / 6 h / Heating

With triethylsilane; aluminium trichloride; trifluoroacetic acid; In dichloromethane; 1: Friedel-Crafts acylation;
DOI:10.1021/jm000491y

Reference yield:

: 332012-05-2
(S)-(-)-N-trifluoroacetyl-1-(2,3,6,7-tetrahydrobenzo[1,2-b;4,5-b']difuran-4-yl)-2-aminopropane

: 219986-75-1
(S)-(+)-1-(8-bromo-2,3,6,7-tetrahydrobenzo[1,2-b;4,5-b']difuran-4-yl)-2-aminopropane

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / Br₂ / acetic acid / 4.5 h / 20 °C

2: aq. 5 N NaOH / methanol

With sodium hydroxide; bromine; In methanol; acetic acid;
DOI:10.1021/jm000491y