N-(4-chlorophenyl)-5-(2-(5-((((1-ethyl-1H-1,2,3-triazol-4-yl)methyl)(isopropyl)amino)methyl)pyridin-2-yl)thieno[3,2-b]pyridin-7-yloxy)benzo[d]oxazol-2-amine

Base Information

Chemical Name:N-(4-chlorophenyl)-5-(2-(5-((((1-ethyl-1H-1,2,3-triazol-4-yl)methyl)(isopropyl)amino)methyl)pyridin-2-yl)thieno[3,2-b]pyridin-7-yloxy)benzo[d]oxazol-2-amine
CAS No.:1430330-90-7
Molecular Formula:C₃₄H₃₁ClN₈O₂S
Molecular Weight:651.192
Hs Code.:

N-(4-chlorophenyl)-5-(2-(5-((((1-ethyl-1H-1,2,3-triazol-4-yl)methyl)(isopropyl)amino)methyl)pyridin-2-yl)thieno[3,2-b]pyridin-7-yloxy)benzo[d]oxazol-2-amine

Synonyms:N-(4-chlorophenyl)-5-(2-(5-((((1-ethyl-1H-1,2,3-triazol-4-yl)methyl)(isopropyl)amino)methyl)pyridin-2-yl)thieno[3,2-b]pyridin-7-yloxy)benzo[d]oxazol-2-amine

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Chemical Property of N-(4-chlorophenyl)-5-(2-(5-((((1-ethyl-1H-1,2,3-triazol-4-yl)methyl)(isopropyl)amino)methyl)pyridin-2-yl)thieno[3,2-b]pyridin-7-yloxy)benzo[d]oxazol-2-amine

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Technology Process of N-(4-chlorophenyl)-5-(2-(5-((((1-ethyl-1H-1,2,3-triazol-4-yl)methyl)(isopropyl)amino)methyl)pyridin-2-yl)thieno[3,2-b]pyridin-7-yloxy)benzo[d]oxazol-2-amine

There total 8 articles about N-(4-chlorophenyl)-5-(2-(5-((((1-ethyl-1H-1,2,3-triazol-4-yl)methyl)(isopropyl)amino)methyl)pyridin-2-yl)thieno[3,2-b]pyridin-7-yloxy)benzo[d]oxazol-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 1430331-49-9
N-(4-chlorophenyl)-5-(2-(5-((prop-2-ynylamino)methyl)pyridin-2-yl)thieno[3,2-b]pyridin-7-yloxy)benzo[d]oxazol-2-amine

: 75-03-6
ethyl iodide

: 1430330-90-7
N-(4-chlorophenyl)-5-(2-(5-((((1-ethyl-1H-1,2,3-triazol-4-yl)methyl)(isopropyl)amino)methyl)pyridin-2-yl)thieno[3,2-b]pyridin-7-yloxy)benzo[d]oxazol-2-amine

Guidance literature:: ethyl iodide; With sodium azide; In dimethyl sulfoxide; at 20 ℃; for 2h;

N-(4-chlorophenyl)-5-(2-(5-((prop-2-ynylamino)methyl)pyridin-2-yl)thieno[3,2-b]pyridin-7-yloxy)benzo[d]oxazol-2-amine; With copper diacetate; sodium L-ascorbate; In dimethyl sulfoxide; for 1h;

Reference yield:

: 1430331-35-3
3-(3-(4-Chlorophenyl)thioureido)-4-hydroxyphenyl benzoate

: 1430330-90-7
N-(4-chlorophenyl)-5-(2-(5-((((1-ethyl-1H-1,2,3-triazol-4-yl)methyl)(isopropyl)amino)methyl)pyridin-2-yl)thieno[3,2-b]pyridin-7-yloxy)benzo[d]oxazol-2-amine

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / Reflux

2.1: methanol; potassium carbonate / tetrahydrofuran / 2 h / 20 °C

3.1: potassium tert-butylate / dimethyl sulfoxide / 1 h / 20 - 90 °C

4.1: hydrogenchloride / tetrahydrofuran; water / 3 h / 20 - 50 °C

5.1: dibutyltin chloride; phenylsilane / ethyl acetate; N,N-dimethyl-formamide / 20 °C

6.1: sodium azide / dimethyl sulfoxide / 2 h / 20 °C

6.2: 1 h

With hydrogenchloride; methanol; sodium azide; phenylsilane; dibutyltin chloride; potassium tert-butylate; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 1430331-41-1
5-(2-(5-(1,3-dioxolan-2-yl)pyridin-2-yl)thieno[3,2-b]pyridin-7-yloxy)-N-(4-chlorophenyl)benzo[d]oxazol-2-amine

: 1430330-90-7
N-(4-chlorophenyl)-5-(2-(5-((((1-ethyl-1H-1,2,3-triazol-4-yl)methyl)(isopropyl)amino)methyl)pyridin-2-yl)thieno[3,2-b]pyridin-7-yloxy)benzo[d]oxazol-2-amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride / tetrahydrofuran; water / 3 h / 20 - 50 °C

2.1: dibutyltin chloride; phenylsilane / ethyl acetate; N,N-dimethyl-formamide / 20 °C

3.1: sodium azide / dimethyl sulfoxide / 2 h / 20 °C

3.2: 1 h

With hydrogenchloride; sodium azide; phenylsilane; dibutyltin chloride; In tetrahydrofuran; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;