octa(2-cyanoethyl) 2,5-di-O-benzyl-myo-inositol 1,3,4,6-tetrakisphosphate

Base Information

Chemical Name:octa(2-cyanoethyl) 2,5-di-O-benzyl-myo-inositol 1,3,4,6-tetrakisphosphate
CAS No.:142409-35-6
Molecular Formula:C₄₄H₅₂N₈O₁₈P₄
Molecular Weight:1104.83
Hs Code.:

Synonyms:octa(2-cyanoethyl) 2,5-di-O-benzyl-myo-inositol 1,3,4,6-tetrakisphosphate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of octa(2-cyanoethyl) 2,5-di-O-benzyl-myo-inositol 1,3,4,6-tetrakisphosphate

Chemical Property:

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Technology Process of octa(2-cyanoethyl) 2,5-di-O-benzyl-myo-inositol 1,3,4,6-tetrakisphosphate

There total 10 articles about octa(2-cyanoethyl) 2,5-di-O-benzyl-myo-inositol 1,3,4,6-tetrakisphosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 142387-36-8
Phosphorous acid (1S,2S,3R,4R,5R,6S)-2,5-bis-benzyloxy-3,4,6-tris-[bis-(2-cyano-ethoxy)-phosphanyloxy]-cyclohexyl ester bis-(2-cyano-ethyl) ester

: 142409-35-6
octa(2-cyanoethyl) 2,5-di-O-benzyl-myo-inositol 1,3,4,6-tetrakisphosphate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 1h; Yield given;
DOI:10.1016/S0008-6215(00)90549-4

Reference yield:

: 142387-34-6
1,3,4,6-tetra-O-allyl-2,5-di-O-benzyl-myo-inositol

: 142409-35-6
octa(2-cyanoethyl) 2,5-di-O-benzyl-myo-inositol 1,3,4,6-tetrakisphosphate

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / toluene-p-sulphonic acid / 10percent Pd-C / ethanol; H₂O / 36 h / Heating

2: 1H-tetrazole / acetonitrile; CH₂Cl₂ / 3 h / 20 °C

3: m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / 20 °C

With 1H-tetrazole; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In ethanol; dichloromethane; water; acetonitrile;
DOI:10.1016/S0008-6215(00)90549-4

Reference yield:

: 100-39-0
benzyl bromide

: 142409-35-6
octa(2-cyanoethyl) 2,5-di-O-benzyl-myo-inositol 1,3,4,6-tetrakisphosphate

Guidance literature:: Multi-step reaction with 4 steps

1: NaH / dimethylformamide / 20 °C

2: 80 percent / toluene-p-sulphonic acid / 10percent Pd-C / ethanol; H₂O / 36 h / Heating

3: 1H-tetrazole / acetonitrile; CH₂Cl₂ / 3 h / 20 °C

4: m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / 20 °C

With 1H-tetrazole; sodium hydride; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0008-6215(00)90549-4