Phosphorous acid (1S,2S,3R,4R,5R,6S)-2,5-bis-benzyloxy-3,4,6-tris-[bis-(2-cyano-ethoxy)-phosphanyloxy]-cyclohexyl ester bis-(2-cyano-ethyl) ester

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Chemical Name:Phosphorous acid (1S,2S,3R,4R,5R,6S)-2,5-bis-benzyloxy-3,4,6-tris-[bis-(2-cyano-ethoxy)-phosphanyloxy]-cyclohexyl ester bis-(2-cyano-ethyl) ester
CAS No.:142387-36-8
Molecular Formula:C₄₄H₅₂N₈O₁₄P₄
Molecular Weight:1040.84
Hs Code.:

Synonyms:Phosphorous acid (1S,2S,3R,4R,5R,6S)-2,5-bis-benzyloxy-3,4,6-tris-[bis-(2-cyano-ethoxy)-phosphanyloxy]-cyclohexyl ester bis-(2-cyano-ethyl) ester

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Chemical Property of Phosphorous acid (1S,2S,3R,4R,5R,6S)-2,5-bis-benzyloxy-3,4,6-tris-[bis-(2-cyano-ethoxy)-phosphanyloxy]-cyclohexyl ester bis-(2-cyano-ethyl) ester

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Technology Process of Phosphorous acid (1S,2S,3R,4R,5R,6S)-2,5-bis-benzyloxy-3,4,6-tris-[bis-(2-cyano-ethoxy)-phosphanyloxy]-cyclohexyl ester bis-(2-cyano-ethyl) ester

There total 3 articles about Phosphorous acid (1S,2S,3R,4R,5R,6S)-2,5-bis-benzyloxy-3,4,6-tris-[bis-(2-cyano-ethoxy)-phosphanyloxy]-cyclohexyl ester bis-(2-cyano-ethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 142387-36-8
Phosphorous acid (1S,2S,3R,4R,5R,6S)-2,5-bis-benzyloxy-3,4,6-tris-[bis-(2-cyano-ethoxy)-phosphanyloxy]-cyclohexyl ester bis-(2-cyano-ethyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / dimethylformamide / 20 °C

2: 80 percent / toluene-p-sulphonic acid / 10percent Pd-C / ethanol; H₂O / 36 h / Heating

3: 1H-tetrazole / acetonitrile; CH₂Cl₂ / 3 h / 20 °C

With 1H-tetrazole; sodium hydride; toluene-4-sulfonic acid; palladium on activated charcoal; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0008-6215(00)90549-4

Reference yield:

: 136986-12-4
1,3,4,6-tetra-O-allyl-myo-inositol

: 142387-36-8
Phosphorous acid (1S,2S,3R,4R,5R,6S)-2,5-bis-benzyloxy-3,4,6-tris-[bis-(2-cyano-ethoxy)-phosphanyloxy]-cyclohexyl ester bis-(2-cyano-ethyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / dimethylformamide / 20 °C

2: 80 percent / toluene-p-sulphonic acid / 10percent Pd-C / ethanol; H₂O / 36 h / Heating

3: 1H-tetrazole / acetonitrile; CH₂Cl₂ / 3 h / 20 °C

With 1H-tetrazole; sodium hydride; toluene-4-sulfonic acid; palladium on activated charcoal; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0008-6215(00)90549-4

Reference yield:

: 142387-34-6
1,3,4,6-tetra-O-allyl-2,5-di-O-benzyl-myo-inositol

: 142387-36-8
Phosphorous acid (1S,2S,3R,4R,5R,6S)-2,5-bis-benzyloxy-3,4,6-tris-[bis-(2-cyano-ethoxy)-phosphanyloxy]-cyclohexyl ester bis-(2-cyano-ethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / toluene-p-sulphonic acid / 10percent Pd-C / ethanol; H₂O / 36 h / Heating

2: 1H-tetrazole / acetonitrile; CH₂Cl₂ / 3 h / 20 °C

With 1H-tetrazole; toluene-4-sulfonic acid; palladium on activated charcoal; In ethanol; dichloromethane; water; acetonitrile;
DOI:10.1016/S0008-6215(00)90549-4