dibenzyl {[(2-aminoethyl)azanediyl]bis(ethane-2,1-diyl)}dicarbamate

Base Information

• Chemical Name: dibenzyl {[(2-aminoethyl)azanediyl]bis(ethane-2,1-diyl)}dicarbamate
• CAS No.: 247170-99-6
• Molecular Formula: C₂₂H₃₀N₄O₄
• Molecular Weight: 414.505
• Mol file: 247170-99-6.mol

Synonyms:dibenzyl {[(2-aminoethyl)azanediyl]bis(ethane-2,1-diyl)}dicarbamate

Chemical Property of dibenzyl {[(2-aminoethyl)azanediyl]bis(ethane-2,1-diyl)}dicarbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dibenzyl {[(2-aminoethyl)azanediyl]bis(ethane-2,1-diyl)}dicarbamate

There total 4 articles about dibenzyl {[(2-aminoethyl)azanediyl]bis(ethane-2,1-diyl)}dicarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

2,2',2''-triaminotriethylamine (4097-89-6) + benzyl phenyl carbonate (28170-07-2) → dibenzyl {[(2-aminoethyl)azanediyl]bis(ethane-2,1-diyl)}dicarbamate (247170-99-6)

Guidance literature:

In ethanol; at 0 - 20 ℃;

Reference yield: 72.0%

2,2',2''-triaminotriethylamine (4097-89-6) + N-(benzyloxycarbonyl)aniline (3422-02-4) → dibenzyl {[(2-aminoethyl)azanediyl]bis(ethane-2,1-diyl)}dicarbamate (247170-99-6)

Guidance literature:

In dichloromethane; at 20 ℃; for 12h; Inert atmosphere; Cooling with ice;

Reference yield: 66.0%

2,2',2''-triaminotriethylamine (4097-89-6) + benzylphenyl carbonate → dibenzyl {[(2-aminoethyl)azanediyl]bis(ethane-2,1-diyl)}dicarbamate (247170-99-6)

Guidance literature:

In ethanol; at 20 ℃; Cooling with ice;

DOI:10.3762/bjoc.8.175

upstream raw materials:

dibenzyl tert-butyl(nitrilotris(ethane-2,1-diyl))tricarbamate

2,2',2''-triaminotriethylamine

benzyl phenyl carbonate

N-(benzyloxycarbonyl)aniline

Downstream raw materials:

C₄₁H₅₆N₆O₈

dibenzyl tert-butyl(nitrilotris(ethane-2,1-diyl))tricarbamate