N⁶-benzyloxycarbonyl-L-2,6-diaminopimelamic acid

Base Information

Chemical Name:N⁶-benzyloxycarbonyl-L-2,6-diaminopimelamic acid
CAS No.:78082-26-5
Molecular Formula:C₁₅H₂₁N₃O₅
Molecular Weight:323.349
Hs Code.:

N<sup>6</sup>-benzyloxycarbonyl-L-2,6-diaminopimelamic acid

Synonyms:N⁶-benzyloxycarbonyl-L-2,6-diaminopimelamic acid

Suppliers and Price of N⁶-benzyloxycarbonyl-L-2,6-diaminopimelamic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N⁶-benzyloxycarbonyl-L-2,6-diaminopimelamic acid

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

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Technology Process of N⁶-benzyloxycarbonyl-L-2,6-diaminopimelamic acid

There total 13 articles about N⁶-benzyloxycarbonyl-L-2,6-diaminopimelamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 121190-51-0
O¹-p-nitrobenzyl-N²-benzyloxycarbonyl-L-2,6-diaminopimelic acid

: 78082-26-5
N⁶-benzyloxycarbonyl-L-2,6-diaminopimelamic acid

Guidance literature:: With ammonium hydroxide; In ethyl acetate; at 20 ℃; for 24h;

Reference yield:

: 41980-31-8
2,6-dicyanopiperidine

: 78082-26-5
N⁶-benzyloxycarbonyl-L-2,6-diaminopimelamic acid

Guidance literature:: Multi-step reaction with 11 steps

1: 98 percent / ammonium bicarbonate, NH₄OH / 4 h / 100 - 105 °C / autoclave

2: 70 percent / aq. HBr(48percent, d = 1.49) / 36 h / Heating

4: 1.) aq. NaOH, AcOH (pH 5.2), 2.) papain, L-cysteine, KH₂PO₄, Na₂HPO₄ / 2.) water, 24 h, 37 deg C

5: 91 percent / aq. HCl (d = 1.19), AcOH / 24 h / Heating

6: 1.) aq. NaOH (pH 8-9), dicyclohexylamine, 2.) aq. methanesulfonic acid / 1.) 0 deg C --> room temperature, 20 h, 2.) water, EtOAc

7: 89 percent / toluene-p-sulphonic acid / toluene / 5 h / Heating

8: 32 percent / KOH / phenylmethanol / 1.) 40 deg C, 7.5 h, 2.) 20 deg C, 16 h

9: 95 percent / NH₃ / methanol / 144 h / 20 °C / autoclave

10: 99 percent / aq. HCl (d = 1.19), H₂ / palladium-charcoal (3percent) / methanol / 4 h

11: 1.) CuBr₂, aq. NaOH (pH 10 --> 8), 2.) aq. HCl, H₂S (gas) / 1.) water, 20 deg C, 20 h, 2.) MeOH, 22 h

With hydrogenchloride; potassium hydroxide; ammonium hydroxide; sodium hydroxide; disodium hydrogenphosphate; potassium dihydrogenphosphate; methanesulfonic acid; L-Cysteine; hydrogen sulfide; ammonia; hydrogen bromide; hydrogen; ammonium bicarbonate; toluene-4-sulfonic acid; acetic acid; N-cyclohexyl-cyclohexanamine; copper(ll) bromide; papain; palladium on activated charcoal; In methanol; toluene; benzyl alcohol;

Reference yield:

: 41980-32-9
5,5'-trimethylenedihydantoin

: 78082-26-5
N⁶-benzyloxycarbonyl-L-2,6-diaminopimelamic acid

Guidance literature:: Multi-step reaction with 10 steps

1: 70 percent / aq. HBr(48percent, d = 1.49) / 36 h / Heating

3: 1.) aq. NaOH, AcOH (pH 5.2), 2.) papain, L-cysteine, KH₂PO₄, Na₂HPO₄ / 2.) water, 24 h, 37 deg C

4: 91 percent / aq. HCl (d = 1.19), AcOH / 24 h / Heating

5: 1.) aq. NaOH (pH 8-9), dicyclohexylamine, 2.) aq. methanesulfonic acid / 1.) 0 deg C --> room temperature, 20 h, 2.) water, EtOAc

6: 89 percent / toluene-p-sulphonic acid / toluene / 5 h / Heating

7: 32 percent / KOH / phenylmethanol / 1.) 40 deg C, 7.5 h, 2.) 20 deg C, 16 h

8: 95 percent / NH₃ / methanol / 144 h / 20 °C / autoclave

9: 99 percent / aq. HCl (d = 1.19), H₂ / palladium-charcoal (3percent) / methanol / 4 h

10: 1.) CuBr₂, aq. NaOH (pH 10 --> 8), 2.) aq. HCl, H₂S (gas) / 1.) water, 20 deg C, 20 h, 2.) MeOH, 22 h

With hydrogenchloride; potassium hydroxide; sodium hydroxide; disodium hydrogenphosphate; potassium dihydrogenphosphate; methanesulfonic acid; L-Cysteine; hydrogen sulfide; ammonia; hydrogen bromide; hydrogen; toluene-4-sulfonic acid; acetic acid; N-cyclohexyl-cyclohexanamine; copper(ll) bromide; papain; palladium on activated charcoal; In methanol; toluene; benzyl alcohol;