2,2-diphenyl-N-<4-(N'-ethyl-N'-4-methoxybenzyl)amino-2-butynyl>-2-hydroxyacetamide

Base Information

Chemical Name:2,2-diphenyl-N-<4-(N'-ethyl-N'-4-methoxybenzyl)amino-2-butynyl>-2-hydroxyacetamide
CAS No.:144314-08-9
Molecular Formula:C₂₈H₃₀N₂O₃
Molecular Weight:442.558
Hs Code.:

Synonyms:2,2-diphenyl-N-<4-(N'-ethyl-N'-4-methoxybenzyl)amino-2-butynyl>-2-hydroxyacetamide

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Chemical Property of 2,2-diphenyl-N-<4-(N'-ethyl-N'-4-methoxybenzyl)amino-2-butynyl>-2-hydroxyacetamide

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Technology Process of 2,2-diphenyl-N-<4-(N'-ethyl-N'-4-methoxybenzyl)amino-2-butynyl>-2-hydroxyacetamide

There total 3 articles about 2,2-diphenyl-N-<4-(N'-ethyl-N'-4-methoxybenzyl)amino-2-butynyl>-2-hydroxyacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 22993-76-6
N-ethyl-4-methoxybenzenemethanamine

: 131839-44-6
2,2-diphenyl-2-hydroxy-N-propargylacetamide

: 144314-08-9
2,2-diphenyl-N-<4-(N'-ethyl-N'-4-methoxybenzyl)amino-2-butynyl>-2-hydroxyacetamide

Guidance literature:: With copper(l) chloride; In 1,4-dioxane; for 0.5h; Heating;
DOI:10.1248/cpb.40.1415

Reference yield:

: 2-Chloro-2,2-diphenyl-N-prop-2-ynyl-acetamide

: 144314-08-9
2,2-diphenyl-N-<4-(N'-ethyl-N'-4-methoxybenzyl)amino-2-butynyl>-2-hydroxyacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 0.3N aq. HCl / dioxane / 1 h / Heating

2: 96 percent / CuCl / dioxane / 0.5 h / Heating

With hydrogenchloride; copper(l) chloride; In 1,4-dioxane;
DOI:10.1248/cpb.40.1415

Reference yield:

: 2902-98-9
2-chloro-2,2-diphenylacetyl chloride

: 144314-08-9
2,2-diphenyl-N-<4-(N'-ethyl-N'-4-methoxybenzyl)amino-2-butynyl>-2-hydroxyacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CHCl₃ / 0.5 h / Ambient temperature

2: 0.3N aq. HCl / dioxane / 1 h / Heating

3: 96 percent / CuCl / dioxane / 0.5 h / Heating

With hydrogenchloride; triethylamine; copper(l) chloride; In 1,4-dioxane; chloroform;
DOI:10.1248/cpb.40.1415