5-((4-([1,1'-biphenyl]-4-yl)-6-oxo-1,6-dihydropyrimidin-2-yl)thio)pentanoic acid

Base Information

Chemical Name:5-((4-([1,1'-biphenyl]-4-yl)-6-oxo-1,6-dihydropyrimidin-2-yl)thio)pentanoic acid
CAS No.:1023694-81-6
Molecular Formula:C₂₁H₂₀N₂O₃S
Molecular Weight:380.467
Hs Code.:

Synonyms:5-((4-([1,1'-biphenyl]-4-yl)-6-oxo-1,6-dihydropyrimidin-2-yl)thio)pentanoic acid

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Chemical Property of 5-((4-([1,1'-biphenyl]-4-yl)-6-oxo-1,6-dihydropyrimidin-2-yl)thio)pentanoic acid

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Technology Process of 5-((4-([1,1'-biphenyl]-4-yl)-6-oxo-1,6-dihydropyrimidin-2-yl)thio)pentanoic acid

There total 1 articles about 5-((4-([1,1'-biphenyl]-4-yl)-6-oxo-1,6-dihydropyrimidin-2-yl)thio)pentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1023694-73-6
ethyl 5-(4-(biphenyl-4-yl)-6-oxo-1,6-dihydropyrimidin-2-ylthio)pentanoate

: 1023694-81-6
5-((4-([1,1'-biphenyl]-4-yl)-6-oxo-1,6-dihydropyrimidin-2-yl)thio)pentanoic acid

Guidance literature:: With potassium hydroxide; In ethanol; water; at 20 ℃; for 18h;
DOI:10.1016/j.bmcl.2008.03.055

Reference yield: 51.0%

: 1023694-81-6
5-((4-([1,1'-biphenyl]-4-yl)-6-oxo-1,6-dihydropyrimidin-2-yl)thio)pentanoic acid

: 95-54-5
1,2-diamino-benzene

: 1023694-49-6
C₂₇H₂₆N₄O₂S

Guidance literature:: 5-((4-([1,1'-biphenyl]-4-yl)-6-oxo-1,6-dihydropyrimidin-2-yl)thio)pentanoic acid; With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

1,2-diamino-benzene; In N,N-dimethyl-formamide; at 20 ℃; Further stages.;
DOI:10.1016/j.bmcl.2008.03.055

Reference yield: 47.0%

: 1023694-81-6
5-((4-([1,1'-biphenyl]-4-yl)-6-oxo-1,6-dihydropyrimidin-2-yl)thio)pentanoic acid

: 479-27-6
naphthalene-1,8-diamine

: 1023694-51-0
C₃₁H₂₈N₄O₂S

Guidance literature:: 5-((4-([1,1'-biphenyl]-4-yl)-6-oxo-1,6-dihydropyrimidin-2-yl)thio)pentanoic acid; With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

naphthalene-1,8-diamine; In N,N-dimethyl-formamide; at 20 ℃; Further stages.;
DOI:10.1016/j.bmcl.2008.03.055