N-4-methoxybenzyl-2-bromo-N-(cyclohexylidenemethyl)-2-methylpropanamide

Base Information

Chemical Name:N-4-methoxybenzyl-2-bromo-N-(cyclohexylidenemethyl)-2-methylpropanamide
CAS No.:360559-05-3
Molecular Formula:C₁₉H₂₆BrNO₂
Molecular Weight:380.325
Hs Code.:

Synonyms:N-4-methoxybenzyl-2-bromo-N-(cyclohexylidenemethyl)-2-methylpropanamide

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Chemical Property of N-4-methoxybenzyl-2-bromo-N-(cyclohexylidenemethyl)-2-methylpropanamide

Chemical Property:

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Technology Process of N-4-methoxybenzyl-2-bromo-N-(cyclohexylidenemethyl)-2-methylpropanamide

There total 3 articles about N-4-methoxybenzyl-2-bromo-N-(cyclohexylidenemethyl)-2-methylpropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20769-85-1
2-bromoisobutyric acid bromide

: 219915-83-0
[1-Cyclohexyl-meth-(E)-ylidene]-(4-methoxy-benzyl)-amine

: 360559-05-3
N-4-methoxybenzyl-2-bromo-N-(cyclohexylidenemethyl)-2-methylpropanamide

Guidance literature:: 2-bromoisobutyric acid bromide; [1-Cyclohexyl-meth-(E)-ylidene]-(4-methoxy-benzyl)-amine; In toluene; at 0 - 20 ℃; for 1h;

With triethylamine; In toluene; at 0 - 20 ℃; for 2h;
DOI:10.1016/S0040-4020(03)01030-5

Reference yield:

: 2393-23-9
4-methoxy-benzylamine

: 360559-05-3
N-4-methoxybenzyl-2-bromo-N-(cyclohexylidenemethyl)-2-methylpropanamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene / Heating

2.1: toluene / 1 h / 0 - 20 °C

2.2: 3.52 g / triethylamine / toluene / 2 h / 0 - 20 °C

In toluene;
DOI:10.1016/S0040-4020(03)01030-5

Reference yield:

: 2043-61-0
cyclohexanecarbaldehyde

: 360559-05-3
N-4-methoxybenzyl-2-bromo-N-(cyclohexylidenemethyl)-2-methylpropanamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene / Heating

2.1: toluene / 1 h / 0 - 20 °C

2.2: 3.52 g / triethylamine / toluene / 2 h / 0 - 20 °C

In toluene;
DOI:10.1016/S0040-4020(03)01030-5