5-pentanoyl-(S)-O-tert-butylaspartyl-(S)-O-tert-butylphenylalanyl

Base Information

Chemical Name:5-pentanoyl-(S)-O-tert-butylaspartyl-(S)-O-tert-butylphenylalanyl
CAS No.:150465-62-6
Molecular Formula:C₃₃H₄₇N₃O₆
Molecular Weight:581.753
Hs Code.:

5-<p-(aminomethyl)phenyl>pentanoyl-(S)-O-tert-butylaspartyl-(S)-O-tert-butylphenylalanyl

Synonyms:5-pentanoyl-(S)-O-tert-butylaspartyl-(S)-O-tert-butylphenylalanyl

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Chemical Property of 5-pentanoyl-(S)-O-tert-butylaspartyl-(S)-O-tert-butylphenylalanyl

Chemical Property:

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Technology Process of 5-pentanoyl-(S)-O-tert-butylaspartyl-(S)-O-tert-butylphenylalanyl

There total 4 articles about 5-pentanoyl-(S)-O-tert-butylaspartyl-(S)-O-tert-butylphenylalanyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (S)-N-((S)-1-tert-Butoxycarbonyl-2-phenyl-ethyl)-3-[5-(4-cyano-phenyl)-pent-4-ynoylamino]-succinamic acid tert-butyl ester

: 150465-62-6
5-pentanoyl-(S)-O-tert-butylaspartyl-(S)-O-tert-butylphenylalanyl

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; In methanol; for 4h; under 3102.9 Torr;
DOI:10.1021/jm00065a003

Reference yield:

: 6089-09-4
4-pentynoic acid

: 150465-62-6
5-pentanoyl-(S)-O-tert-butylaspartyl-(S)-O-tert-butylphenylalanyl

Guidance literature:: Multi-step reaction with 3 steps

1: 3P>4Pd, piperidine / 1.5 h / 80 °C

2: N,N-dicyclohexylcarbodiimide (DCC) / CH₂Cl₂ / 20 h / 23 °C

3: 750 mg / H₂, 1 N HCl / 10percent Pd/C / methanol / 4 h / 3102.9 Torr

With piperidine; hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/jm00065a003

Reference yield:

: 623-00-7
4-bromobenzenecarbonitrile

: 150465-62-6
5-pentanoyl-(S)-O-tert-butylaspartyl-(S)-O-tert-butylphenylalanyl

Guidance literature:: Multi-step reaction with 3 steps

1: 3P>4Pd, piperidine / 1.5 h / 80 °C

2: N,N-dicyclohexylcarbodiimide (DCC) / CH₂Cl₂ / 20 h / 23 °C

3: 750 mg / H₂, 1 N HCl / 10percent Pd/C / methanol / 4 h / 3102.9 Torr

With piperidine; hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/jm00065a003